Pei Y H, Li X, Zhu T R
Yao Xue Xue Bao. 1989;24(6):431-7.
Five compounds were isolated from the petroleum ether extract of the root-sprouts of Agrimonia pilosa Ledob. A new compound, (R)-(-)-agrimol B (III), was elucidated by means of physical and chemical properties, spectroscopy (MS, IR, PMR, UV) and total synthesis. Four known compounds were identified as agrimophol (I), n-nonacosane (II), beta-sitosterol (IV) and pseudo-aspidin (V), the last one being previously known only as a synthetic entity. (S)-(+)-Agrimol B also was synthesized.
从龙牙草根芽的石油醚提取物中分离出了5种化合物。通过物理和化学性质、光谱学(质谱、红外光谱、质子磁共振谱、紫外光谱)以及全合成,阐明了一种新化合物,即(R)-(-)-仙鹤草酚B(III)。鉴定出4种已知化合物,分别为仙鹤草甲素(I)、正二十九烷(II)、β-谷甾醇(IV)和伪绵马素(V),最后一种化合物此前仅作为合成物为人所知。还合成了(S)-(+)-仙鹤草酚B。