Kvashnina Kristina O, Scheinost Andreas C
Rossendorf Beamline at ESRF - The European Synchrotron, CS40220, 38043 Grenoble Cedex 9, France.
J Synchrotron Radiat. 2016 May;23(Pt 3):836-41. doi: 10.1107/S1600577516004483. Epub 2016 Apr 16.
This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.
本文详细描述了一种约翰型X射线发射光谱仪,包括相关方程。该光谱仪最近已在欧洲同步辐射装置的罗斯多夫光束线(ROBL)上安装并进行了测试。该光谱仪由一个单球形弯曲晶体分析仪和一个雪崩光电二极管探测器组成,探测器位于直径为1 m的垂直罗兰圆上。硬X射线发射光谱仪(~3.5 - 25 keV)在大气压下运行,覆盖65° - 89°的布拉格角。该仪器已在ROBL的第二个实验小屋中,在高和中等入射能量下进行了测试,即在锆K边和金L3边进行了测试。该光谱仪专门用于通过高能量分辨率X射线吸收和X射线发射光谱研究材料和环境样品中的锕系元素。