• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

用于NSLS-II内壳层光谱光束线硬X射线光子入/光子出光谱分析的五分析仪约翰光谱仪:设计、对准与数据采集

Five-analyzer Johann spectrometer for hard X-ray photon-in/photon-out spectroscopy at the Inner Shell Spectroscopy beamline at NSLS-II: design, alignment and data acquisition.

作者信息

Tayal Akhil, Coburn David Scott, Abel Donald, Rakitin Max, Ivashkevych Oksana, Wlodek Jakub, Wierzbicki Dominik, Xu Weihe, Nazaretski Evgeny, Stavitski Eli, Leshchev Denis

机构信息

National Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.

出版信息

J Synchrotron Radiat. 2024 Nov 1;31(Pt 6):1609-1621. doi: 10.1107/S1600577524009342. Epub 2024 Oct 30.

DOI:10.1107/S1600577524009342
PMID:39475836
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11542649/
Abstract

Here, a recently commissioned five-analyzer Johann spectrometer at the Inner Shell Spectroscopy beamline (8-ID) at the National Synchrotron Light Source II (NSLS-II) is presented. Designed for hard X-ray photon-in/photon-out spectroscopy, the spectrometer achieves a resolution in the 0.5-2 eV range, depending on the element and/or emission line, providing detailed insights into the local electronic and geometric structure of materials. It serves a diverse user community, including fields such as physical, chemical, biological, environmental and materials sciences. This article details the mechanical design, alignment procedures and data-acquisition scheme of the spectrometer, with a particular focus on the continuous asynchronous data-acquisition approach that significantly enhances experimental efficiency.

摘要

本文介绍了一台最近在国家同步辐射光源II(NSLS-II)的内壳层光谱光束线(8-ID)上投入使用的五分析器约翰光谱仪。该光谱仪专为硬X射线光子入射/光子出射光谱设计,根据元素和/或发射线的不同,其分辨率在0.5 - 2 eV范围内,能够深入了解材料的局部电子和几何结构。它服务于包括物理、化学、生物、环境和材料科学等领域在内的多样化用户群体。本文详细介绍了该光谱仪的机械设计、对准程序和数据采集方案,特别关注了显著提高实验效率的连续异步数据采集方法。

相似文献

1
Five-analyzer Johann spectrometer for hard X-ray photon-in/photon-out spectroscopy at the Inner Shell Spectroscopy beamline at NSLS-II: design, alignment and data acquisition.用于NSLS-II内壳层光谱光束线硬X射线光子入/光子出光谱分析的五分析仪约翰光谱仪:设计、对准与数据采集
J Synchrotron Radiat. 2024 Nov 1;31(Pt 6):1609-1621. doi: 10.1107/S1600577524009342. Epub 2024 Oct 30.
2
Five-element Johann-type x-ray emission spectrometer with a single-photon-counting pixel detector.采用单光子计数像素探测器的五元素约翰型X射线发射光谱仪。
Rev Sci Instrum. 2011 Jun;82(6):065107. doi: 10.1063/1.3600452.
3
The Inner Shell Spectroscopy beamline at NSLS-II: a facility for in situ and operando X-ray absorption spectroscopy for materials research.NSLS-II的内壳层光谱光束线:一个用于材料研究的原位和操作X射线吸收光谱的设施。
J Synchrotron Radiat. 2022 Jul 1;29(Pt 4):1095-1106. doi: 10.1107/S160057752200460X. Epub 2022 May 26.
4
A Johann-type X-ray emission spectrometer at the Rossendorf beamline.位于罗斯多夫光束线的一台约翰型X射线发射光谱仪。
J Synchrotron Radiat. 2016 May;23(Pt 3):836-41. doi: 10.1107/S1600577516004483. Epub 2016 Apr 16.
5
Photon-in/photon-out spectroscopy at the I20-scanning beamline at diamond light source.在钻石光源的I20扫描光束线上进行的光子入射/光子出射光谱分析。
J Phys Condens Matter. 2021 Jun 4;33(28). doi: 10.1088/1361-648X/abfe93.
6
The CLEAR X-ray emission spectrometer available at the CLAESS beamline of ALBA synchrotron.可在 ALBA 同步加速器 CLAESS 光束线上使用的 CLEAR X 射线发射光谱仪。
J Synchrotron Radiat. 2023 Jan 1;30(Pt 1):235-241. doi: 10.1107/S1600577522009821.
7
High energy resolution five-crystal spectrometer for high quality fluorescence and absorption measurements on an x-ray absorption spectroscopy beamline.用于在X射线吸收光谱束线进行高质量荧光和吸收测量的高能量分辨率五晶体光谱仪。
Rev Sci Instrum. 2012 Jun;83(6):063104. doi: 10.1063/1.4728414.
8
Characterization of the soft X-ray spectrometer PEAXIS at BESSY II.PEAXIS 软 X 射线谱仪在 BESSY II 上的特性描述。
J Synchrotron Radiat. 2020 Jan 1;27(Pt 1):238-249. doi: 10.1107/S1600577519014887.
9
Soft X-ray spectroscopy with transition-edge sensors at Stanford Synchrotron Radiation Lightsource beamline 10-1.在斯坦福同步辐射光源10-1光束线使用过渡边传感器进行软X射线光谱分析。
Rev Sci Instrum. 2019 Nov 1;90(11):113101. doi: 10.1063/1.5119155.
10
Performance of a collimating L-shaped laterally graded multilayer mirror for the IXS analyzer system at NSLS-II.用于NSLS-II的IXS分析仪系统的准直L形横向渐变多层镜的性能。
J Synchrotron Radiat. 2014 May;21(Pt 3):473-8. doi: 10.1107/S1600577514002999. Epub 2014 Mar 12.

引用本文的文献

1
Comparison of Single Atoms vs. Sub-Nanoclusters as Co-Catalysts in Perovskites and Metal Oxides for Photocatalytic Technologies.单原子与亚纳米团簇作为钙钛矿和金属氧化物光催化技术共催化剂的比较
Nanomaterials (Basel). 2025 Jan 30;15(3):226. doi: 10.3390/nano15030226.
2
A general Bayesian algorithm for the autonomous alignment of beamlines.一种用于束线自动对准的通用贝叶斯算法。
J Synchrotron Radiat. 2024 Nov 1;31(Pt 6):1446-1456. doi: 10.1107/S1600577524008993. Epub 2024 Oct 28.

本文引用的文献

1
High-Energy-Resolution X-ray Spectroscopy of Evolving Cu Nanoparticle Electrocatalysts for CO Reduction.用于CO还原的演化铜纳米颗粒电催化剂的高能分辨X射线光谱
J Am Chem Soc. 2023 Sep 20;145(37):20208-20213. doi: 10.1021/jacs.3c08182. Epub 2023 Sep 7.
2
Ferricyanide photo-aquation pathway revealed by combined femtosecond Kβ main line and valence-to-core x-ray emission spectroscopy.亚铁氰化物光水合途径的揭示:飞秒 Kβ 主线和价态到芯层 X 射线发射光谱学的联合应用。
Nat Commun. 2023 May 5;14(1):2443. doi: 10.1038/s41467-023-37922-x.
3
A new Kirkpatrick-Baez-based scanning microscope for the Submicron Resolution X-ray Spectroscopy (SRX) beamline at NSLS-II.
一种用于NSLS-II的亚微米分辨率X射线光谱(SRX)光束线的新型基于柯克帕特里克-贝兹的扫描显微镜。
J Synchrotron Radiat. 2022 Sep 1;29(Pt 5):1284-1291. doi: 10.1107/S1600577522007056. Epub 2022 Jul 29.
4
A new μ-high energy resolution fluorescence detection microprobe imaging spectrometer at the Stanford Synchrotron Radiation Lightsource beamline 6-2.斯坦福同步辐射光源光束线 6-2 上的新型 μ-超高能量分辨率荧光探测微探针成像光谱仪
Rev Sci Instrum. 2022 Aug 1;93(8):083101. doi: 10.1063/5.0095229.
5
The Inner Shell Spectroscopy beamline at NSLS-II: a facility for in situ and operando X-ray absorption spectroscopy for materials research.NSLS-II的内壳层光谱光束线:一个用于材料研究的原位和操作X射线吸收光谱的设施。
J Synchrotron Radiat. 2022 Jul 1;29(Pt 4):1095-1106. doi: 10.1107/S160057752200460X. Epub 2022 May 26.
6
Photon-in/photon-out spectroscopy at the I20-scanning beamline at diamond light source.在钻石光源的I20扫描光束线上进行的光子入射/光子出射光谱分析。
J Phys Condens Matter. 2021 Jun 4;33(28). doi: 10.1088/1361-648X/abfe93.
7
Probing Physical Oxidation State by Resonant X-ray Emission Spectroscopy: Applications to Iron Model Complexes and Nitrogenase.共振 X 射线发射光谱法探测物理氧化态:在铁模型配合物和固氮酶中的应用。
Angew Chem Int Ed Engl. 2021 Apr 26;60(18):10112-10121. doi: 10.1002/anie.202015669. Epub 2021 Mar 23.
8
Demethylation of Methylmercury in Bird, Fish, and Earthworm.鸟类、鱼类和蚯蚓中甲基汞的去甲基化。
Environ Sci Technol. 2021 Feb 2;55(3):1527-1534. doi: 10.1021/acs.est.0c04948. Epub 2021 Jan 21.
9
The five-analyzer point-to-point scanning crystal spectrometer at ESRF ID26.欧洲同步辐射装置(ESRF)ID26光束线站的五分析器逐点扫描晶体光谱仪。
J Synchrotron Radiat. 2021 Jan 1;28(Pt 1):362-371. doi: 10.1107/S1600577520015416.
10
New reflections on hard X-ray photon-in/photon-out spectroscopy.硬X射线光子输入/光子输出光谱学的新思考。
Nanoscale. 2020 Aug 14;12(30):16270-16284. doi: 10.1039/d0nr01983f. Epub 2020 Jul 28.