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[一种从尸体标本中分离吩噻嗪衍生物的快速方法]

[A rapid method of isolating a phenothiazine derivatives from cadaveric specimens].

作者信息

Salomatin E M

出版信息

Sud Med Ekspert. 1989 Jan-Mar;32(1):39-41.

PMID:2728067
Abstract

Proximate method for isolation of 10 psychotropic compounds of phenothiazine series from the cadaveric material was developed using acetonitrile with subsequent extraction of these derivatives by ether at pH 13.0 and reextraction by 0.5 n. solution of sulfuric acid. Method of isolation by acetonitrile shortens time for analysis by 5-6 times as compared with modified Stas-Otto method suggested previously for this purpose.

摘要

开发了一种从尸体材料中分离吩噻嗪系列10种精神药物化合物的近似方法,该方法使用乙腈,随后在pH 13.0条件下用乙醚萃取这些衍生物,并用0.5N硫酸溶液进行再萃取。与先前为此目的建议的改良Stas-Otto方法相比,乙腈分离法将分析时间缩短了5至6倍。

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