2-氨基乙磺酸的合成。一种新的伯胺合成方法。
Synthesis of 2-aminoethylarsonic acid. A new synthesis of primary.
作者信息
Geoghegan K F, Dixon H B
机构信息
Department of Biochemistry, University of Cambridge, U.K.
出版信息
Biochem J. 1989 May 15;260(1):295-6. doi: 10.1042/bj2600295.
Abstract
2-Aminoethylarsonic acid was prepared from 2-choloethylarsonic acid. The route constitutes a new procedure for making primary amines from haloalkanes; chloride was displaced by treatment with 2-aminoethanol at 70 degrees C, and the product was converted into the required primary amine by treatment with periodate.
摘要
2-氨基乙胂酸由2-氯乙胂酸制备而成。该路线构成了一种从卤代烷制备伯胺的新方法；通过在70℃下用2-氨基乙醇处理来取代氯，然后用高碘酸盐处理将产物转化为所需的伯胺。
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本文引用的文献
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Detection of phosphate esters on paper chromatograms.纸色谱图上磷酸酯的检测
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Biochem J. 1989 May 15;260(1):296-7. doi: 10.1042/bj2600296.
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Reversible reductive alkylation of amino groups in proteins.蛋白质中氨基的可逆还原烷基化反应。
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