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3-脱氧-D-苏型己糖醛酸作为副溶血性弧菌O7和O12血清型脂多糖成分的分离与鉴定

Isolation and identification of 3-deoxy-D-threo-hexulosonic acid as a constituent of the lipopolysaccharide of Vibrio parahaemolyticus serotypes O7 and O12.

作者信息

Kondo S, Zähringer U, Rietschel E T, Hisatsune K

机构信息

Forschungsinstitut Borstel, F.R.G.

出版信息

Carbohydr Res. 1989 Jun 1;188:97-104. doi: 10.1016/0008-6215(89)84062-5.

DOI:10.1016/0008-6215(89)84062-5
PMID:2776131
Abstract

Treatment of the lipopolysaccharide of Vibrio parahaemolyticus serotypes O7 and O12 with mild acid gave a compound which, on the basis of chemical analysis, g.l.c.-m.s., and 1H and 13C-n.m.r. spectroscopy, was characterized as 3-deoxy-D-threo-hexulosonic acid and shown to be present as a terminal non-substituted pyranose unit.

摘要

用弱酸处理副溶血性弧菌O7和O12血清型的脂多糖，得到一种化合物。基于化学分析、气相色谱 - 质谱联用以及氢核磁共振和碳 - 13核磁共振光谱，该化合物被鉴定为3 - 脱氧 - D - 苏式 - 己糖醛酸，并显示以末端未取代的吡喃糖单元形式存在。

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