气相色谱/质谱法检测人发中的美沙酮。
Detection of methadone in human hair by gas chromatography/mass spectrometry.
作者信息
Balabanova S, Arnold P J, Brunner H, Luckow V, Wolf H U
机构信息
Department of Forensic Medicine, University of Ulm, Federal Republic of Germany.
出版信息
Z Rechtsmed. 1989;102(8):495-501. doi: 10.1007/BF00200647.
PMID:2800728
Abstract
Determination of methadone in human hair by gas chromatography/mass spectrometry was described. Helium as carrier gas, a 30-m bonded phase-fused silica DB-1 capillary column and splitless injection at 230 degree C temperature were used. The concentrations of methadone and its metabolites were measured in addition by radioimmunoassay (RIA). Both methods GC/MS and RIA showed the presence of methadone in human hair.
摘要
描述了采用气相色谱/质谱法测定人发中的美沙酮。使用氦气作为载气，一根30米长的键合相熔融石英DB-1毛细管柱，并在230℃温度下进行不分流进样。此外，还通过放射免疫分析（RIA）测定了美沙酮及其代谢物的浓度。气相色谱/质谱法和放射免疫分析法均显示人发中存在美沙酮。
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