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中国光源(CLS)软X射线材料微分析站的中能微探针站

Medium-energy microprobe station at the SXRMB of the CLS.

作者信息

Xiao Qunfeng, Maclennan Aimee, Hu Yongfeng, Hackett Mark, Leinweber Peter, Sham Tsun Kong

机构信息

Canadian Light Source, 44 Innovation Boulevard, Saskatoon, SK, Canada S7N 2V3.

Department of Geological Sciences, University of Saskatchewan, Saskatoon, SK, Canada S7N 5E2.

出版信息

J Synchrotron Radiat. 2017 Jan 1;24(Pt 1):333-337. doi: 10.1107/S1600577516017604.

Abstract

Micro-XAFS and chemical imaging techniques have been widely applied for studies of heterogeneously distributed systems, mostly in hard X-ray (>5 keV) or in soft X-ray (<1.5 keV) energies. The microprobe endstation of the SXRMB (soft X-ray microcharacterization beamline) at the Canadian Light Source is optimized at the medium energy (1.7-5 keV), and it has been recently commissioned and is available for general users. The technical design and the performance (energy range, beam size and flux) of the SXRMB microprobe are presented. Examples in chemical imaging and micro-XAFS in the medium energy for important elements such as P, S and Ca for soil and biological samples are highlighted.

摘要

微X射线吸收精细结构光谱(Micro-XAFS)和化学成像技术已广泛应用于非均匀分布体系的研究,主要用于硬X射线(>5 keV)或软X射线(<1.5 keV)能量范围。加拿大光源中心的SXRMB(软X射线微表征光束线)的微探针终端站在中能(1.7 - 5 keV)下进行了优化,最近已完成调试并可供普通用户使用。本文介绍了SXRMB微探针的技术设计和性能(能量范围、束斑尺寸和通量)。重点介绍了在中能条件下对土壤和生物样品中重要元素(如P、S和Ca)进行化学成像和微XAFS的实例。

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