Department of Cellulose and Paper Technology, Faculty of New Technologies and Energy Engineering, Shahid Beheshti University, P.O. Box: 47815-168, Zirab Campus, Iran.
Biotechnology group, Chemical Engineering Faculty, Tarbiat Modares University, P.O. Box: 14115-114, Tehran, Iran.
J Photochem Photobiol B. 2017 Feb;167:36-44. doi: 10.1016/j.jphotobiol.2016.12.025. Epub 2016 Dec 21.
In this study, a rapid green synthesis of the silver nanoparticles (AgNPs) using leaves extract of Convolvulus arvensis was investigated. UV-Visible spectra showed the SPR band at around 430nm which proved the AgNP formation. The reduction of silver ions to nanoparticles was completed within 150min. Particle size analysis verified the formation of AgNPs with average size of 28nm, while their PDI was 0.2. XRD patterns verified the crystalline nature of produced AgNPs. SEM images verified the presence of spherical nanoparticles with no evidence of aggregations. FTIR analysis verified the involvement of the phenolic compounds in AgNP formation. It was found that the biosynthesized AgNPs have the antibacterial activity against human pathogen E. coli. Also, nanoparticles exhibit biofilm degrading activity against both bacterial strains of S. aureus and P. aeruginosa. Furthermore, the synthesized AgNPs prevented the coagulation of blood samples. The accelerated reduction of methylene blue (MB) in the presence of AgNPs with rate constant of 0.108min, confirmed the catalytic potential of nanoparticles.
本研究采用田旋花叶片提取物快速绿色合成了银纳米粒子(AgNPs)。紫外-可见光谱在约 430nm 处显示出 SPR 带,证明了 AgNP 的形成。银离子还原为纳米粒子在 150min 内完成。粒径分析证实了平均粒径为 28nm 的 AgNPs 的形成,而其 PDI 为 0.2。XRD 图谱证实了所制备的 AgNPs 的结晶性质。SEM 图像证实了存在无团聚迹象的球形纳米粒子。FTIR 分析证实了酚类化合物在 AgNP 形成中的参与。结果发现,生物合成的 AgNPs 对人类病原体大肠杆菌具有抗菌活性。此外,纳米粒子对金黄色葡萄球菌和铜绿假单胞菌这两种细菌菌株的生物膜均具有降解活性。此外,合成的 AgNPs 阻止了血液样本的凝结。在 AgNPs 的存在下,亚甲基蓝(MB)的加速还原,其速率常数为 0.108min,证实了纳米粒子的催化潜力。