Shinohara Ayano, Taira Yohsuke, Sawase Takashi
Department of Applied Prosthodontics, Graduate School of Biomedical Sciences, Nagasaki University, 1-7-1 Sakamoto, Nagasaki, 852-8588, Japan.
Odontology. 2017 Oct;105(4):437-442. doi: 10.1007/s10266-016-0288-8. Epub 2017 Jan 9.
The present study was conducted to evaluate the effects of an experimental adhesive agent [methyl methacrylate-tributylborane liquid (MT)] and two adhesive agents containing silane on the bonding between a resin composite block of a computer-aided design and manufacturing (CAD/CAM) system and a light-curing resin composite veneering material. The surfaces of CAD/CAM resin composite specimens were ground with silicon-carbide paper, treated with phosphoric acid, and then primed with either one of the two silane agents [Scotchbond Universal Adhesive (SC) and GC Ceramic Primer II (GC)], no adhesive control (Cont), or one of three combinations (MT/SC, MT/GC, and MT/Cont). A light-curing resin composite was veneered on the primed CAD/CAM resin composite surface. The veneered specimens were subjected to thermocycling between 4 and 60 °C for 10,000 cycles, and the shear bond strengths were determined. All data were analyzed using analysis of variance and a post hoc Tukey-Kramer HSD test (α = 0.05, n = 8). MT/SC (38.7 MPa) exhibited the highest mean bond strengths, followed by MT/GC (30.4 MPa), SC (27.9 MPa), and MT/Cont (25.7 MPa), while Cont (12.9 MPa) and GC (12.3 MPa) resulted in the lowest bond strengths. The use of MT in conjunction with a silane agent significantly improved the bond strength. Surface treatment with appropriate adhesive agents was confirmed as a prerequisite for veneering CAD/CAM resin composite restorations.
本研究旨在评估一种实验性粘合剂[甲基丙烯酸甲酯-三丁基硼烷液体(MT)]和两种含硅烷的粘合剂对计算机辅助设计与制造(CAD/CAM)系统的树脂复合材料块与光固化树脂复合贴面材料之间粘结的影响。CAD/CAM树脂复合材料标本的表面用碳化硅纸打磨,用磷酸处理,然后用两种硅烷试剂之一[Scotchbond通用粘合剂(SC)和GC陶瓷底漆II(GC)]、无粘合剂对照(Cont)或三种组合之一(MT/SC、MT/GC和MT/Cont)进行底漆处理。在底漆处理过的CAD/CAM树脂复合材料表面贴上光固化树脂复合材料。将贴有贴面的标本在4至60°C之间进行10000次热循环,并测定剪切粘结强度。所有数据均采用方差分析和事后Tukey-Kramer HSD检验进行分析(α = 0.05,n = 8)。MT/SC(38.7MPa)表现出最高的平均粘结强度,其次是MT/GC(30.4MPa)、SC(27.9MPa)和MT/Cont(25.7MPa),而Cont(12.9MPa)和GC(12.3MPa)的粘结强度最低。MT与硅烷试剂联合使用可显著提高粘结强度。证实使用适当的粘合剂进行表面处理是CAD/CAM树脂复合材料修复体贴面的先决条件。