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三丁基硼烷活化粘合剂和两种硅烷试剂对粘结计算机辅助设计与制造(CAD/CAM)树脂复合材料的影响。

Effects of tributylborane-activated adhesive and two silane agents on bonding computer-aided design and manufacturing (CAD/CAM) resin composite.

作者信息

Shinohara Ayano, Taira Yohsuke, Sawase Takashi

机构信息

Department of Applied Prosthodontics, Graduate School of Biomedical Sciences, Nagasaki University, 1-7-1 Sakamoto, Nagasaki, 852-8588, Japan.

出版信息

Odontology. 2017 Oct;105(4):437-442. doi: 10.1007/s10266-016-0288-8. Epub 2017 Jan 9.

Abstract

The present study was conducted to evaluate the effects of an experimental adhesive agent [methyl methacrylate-tributylborane liquid (MT)] and two adhesive agents containing silane on the bonding between a resin composite block of a computer-aided design and manufacturing (CAD/CAM) system and a light-curing resin composite veneering material. The surfaces of CAD/CAM resin composite specimens were ground with silicon-carbide paper, treated with phosphoric acid, and then primed with either one of the two silane agents [Scotchbond Universal Adhesive (SC) and GC Ceramic Primer II (GC)], no adhesive control (Cont), or one of three combinations (MT/SC, MT/GC, and MT/Cont). A light-curing resin composite was veneered on the primed CAD/CAM resin composite surface. The veneered specimens were subjected to thermocycling between 4 and 60 °C for 10,000 cycles, and the shear bond strengths were determined. All data were analyzed using analysis of variance and a post hoc Tukey-Kramer HSD test (α = 0.05, n = 8). MT/SC (38.7 MPa) exhibited the highest mean bond strengths, followed by MT/GC (30.4 MPa), SC (27.9 MPa), and MT/Cont (25.7 MPa), while Cont (12.9 MPa) and GC (12.3 MPa) resulted in the lowest bond strengths. The use of MT in conjunction with a silane agent significantly improved the bond strength. Surface treatment with appropriate adhesive agents was confirmed as a prerequisite for veneering CAD/CAM resin composite restorations.

摘要

本研究旨在评估一种实验性粘合剂[甲基丙烯酸甲酯-三丁基硼烷液体(MT)]和两种含硅烷的粘合剂对计算机辅助设计与制造(CAD/CAM)系统的树脂复合材料块与光固化树脂复合贴面材料之间粘结的影响。CAD/CAM树脂复合材料标本的表面用碳化硅纸打磨,用磷酸处理,然后用两种硅烷试剂之一[Scotchbond通用粘合剂(SC)和GC陶瓷底漆II(GC)]、无粘合剂对照(Cont)或三种组合之一(MT/SC、MT/GC和MT/Cont)进行底漆处理。在底漆处理过的CAD/CAM树脂复合材料表面贴上光固化树脂复合材料。将贴有贴面的标本在4至60°C之间进行10000次热循环,并测定剪切粘结强度。所有数据均采用方差分析和事后Tukey-Kramer HSD检验进行分析(α = 0.05,n = 8)。MT/SC(38.7MPa)表现出最高的平均粘结强度,其次是MT/GC(30.4MPa)、SC(27.9MPa)和MT/Cont(25.7MPa),而Cont(12.9MPa)和GC(12.3MPa)的粘结强度最低。MT与硅烷试剂联合使用可显著提高粘结强度。证实使用适当的粘合剂进行表面处理是CAD/CAM树脂复合材料修复体贴面的先决条件。

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