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用于二维应变测量的STEM莫尔条纹分析。

STEM moiré analysis for 2D strain measurements.

作者信息

Ishizuka Akimitsu, Hytch Martin, Ishizuka Kazuo

机构信息

HREM Research Inc., Higashimatsuyama 355-0055 , Japan.

CEMES-CNRS and Université de Toulouse, Toulouse 31055 , France.

出版信息

Microscopy (Oxf). 2017 Jun 1;66(3):217-221. doi: 10.1093/jmicro/dfx009.

Abstract

A moiré pattern is created in a scanning transmission electron microscope (STEM) when the scan step is close to a crystalline periodicity. Usually, fringes are visible in only one direction, corresponding to a single set of lattice planes, but fringes can be formed in two directions or more. Using an accurate independent calibration, the strains in silicon devices have been determined from the spacing and orientation of one-directional STEM moiré fringes. In this report, we first discuss the origin of the STEM moiré, and then we show how an accurate calibration of the scan step can be obtained from the STEM moiré pattern itself, providing that we know initially only an approximate scan step and the planar spacing. The new calibration scheme also makes the STEM moiré experiments easier, since it can be applied for the moiré where the scan direction is not precisely aligned with the crystalline lattice. Finally, we show how the two-dimensional strain information will be readily extracted from two one-directional moiré patterns using the concept of geometric phase.

摘要

当扫描步长接近晶体周期性时,扫描透射电子显微镜(STEM)中会产生莫尔条纹图案。通常,条纹仅在一个方向上可见,对应于一组晶格平面,但条纹也可以在两个或更多方向上形成。通过精确的独立校准,已根据单向STEM莫尔条纹的间距和取向确定了硅器件中的应变。在本报告中,我们首先讨论STEM莫尔条纹的起源,然后说明如何从STEM莫尔条纹图案本身获得扫描步长的精确校准,前提是我们最初仅知道近似的扫描步长和平面间距。新的校准方案还使STEM莫尔条纹实验更容易,因为它可应用于扫描方向与晶格未精确对齐的莫尔条纹。最后,我们展示了如何使用几何相位的概念从两个单向莫尔条纹图案中轻松提取二维应变信息。

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