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烧结温度和持续时间对氧化锆抗弯强度和晶粒尺寸的影响。

The effects of sintering temperature and duration on the flexural strength and grain size of zirconia.

作者信息

Ersoy Nuri Murat, Aydoğdu Hasan Murat, Değirmenci Beyza Ünalan, Çökük Neslihan, Sevimay Müjde

机构信息

Faculty of Dentistry, Department of Prosthodontics, Yüzüncü Yıl UniversityVanTurkey.

Faculty of Dentistry, Department of Prosthodontics, Selcuk UniversityKonyaTurkey.

出版信息

Acta Biomater Odontol Scand. 2015 Aug 3;1(2-4):43-50. doi: 10.3109/23337931.2015.1068126. eCollection 2015 Dec.

Abstract

: This study investigated the effect of different sintering temperatures and times on the flexural strength and grain size of zirconia. : Zirconia specimens (In-Coris ZI, In-Coris TZI, 120 samples) were prepared in a partially sintered state. Subsequently, the specimens were randomly divided into three groups and sintered at different final sintering temperatures and for various durations: 1510 °C for 120 min, 1540 °C for 25 min and 1580 °C for 10 min. Three-point flexural strength (for 120 samples, 20 samples per group) was measured according to the ISO 6872: 2008 standards. The grain sizes were imaged by scanning electron microscopy (SEM) and the phase transitions were determined by X-ray diffraction (XRD). The data were analyzed using one-way ANOVA and Duncan tests ( < 0.05). : The highest flexural strength was observed in ZI and TZI samples sintered at 1580 °C for 10 min. The differences between the ZI samples sintered at 1510 °C for 120 min and those sintered at 1540 °C for 25 min were statistically insignificant. Also, TZI samples sintered at 1510 °C for 120 min and those sintered at 1540 °C for 25 min also did not show any statistically significant differences. There were no visible differences in the grain sizes between the ZI and TZI specimens. The XRD patterns indicated similar crystalline structure for both materials subjected to the three different procedures. : The results of this study showed that experimented high sintering temperature and short sintering time combination increases the flexural strength of zirconia.

摘要

本研究调查了不同烧结温度和时间对氧化锆抗弯强度和晶粒尺寸的影响。制备了部分烧结状态的氧化锆试样(In-Coris ZI、In-Coris TZI,共120个样品)。随后,将试样随机分为三组,在不同的最终烧结温度和不同时长下进行烧结:1510℃烧结120分钟、1540℃烧结25分钟、1580℃烧结10分钟。根据ISO 6872:2008标准测量三点抗弯强度(共120个样品,每组20个样品)。通过扫描电子显微镜(SEM)对晶粒尺寸进行成像,并通过X射线衍射(XRD)确定相变。使用单向方差分析和邓肯检验对数据进行分析(P<0.05)。在1580℃烧结10分钟的ZI和TZI样品中观察到最高抗弯强度。在1510℃烧结120分钟的ZI样品和在1540℃烧结25分钟的ZI样品之间的差异无统计学意义。同样,在1510℃烧结120分钟的TZI样品和在1540℃烧结25分钟的TZI样品之间也没有显示出任何统计学上的显著差异。ZI和TZI试样的晶粒尺寸没有明显差异。XRD图谱表明,两种材料在三种不同工艺下的晶体结构相似。本研究结果表明,实验采用的高烧结温度和短烧结时间组合可提高氧化锆的抗弯强度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f324/5433200/82740b3c01e5/iabo_a_1068126_f0001_b.jpg

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