Zhang F G, Bornert M, Petit J, Castelnau O
PIMM CNRS UMR 8006, Arts et Métiers ParisTech, 151 Boulevard de l'Hôpital, 75013 Paris, France.
Laboratoire NAVIER, ENPC/IFSTTAR/CNRS UMR 8205, Université Paris-Est, 77455 Marne-la-Vallée, France.
J Synchrotron Radiat. 2017 Jul 1;24(Pt 4):802-817. doi: 10.1107/S1600577517006622. Epub 2017 Jun 20.
Laue microdiffraction, available at several synchrotron radiation facilities, is well suited for measuring the intragranular stress field in deformed materials thanks to the achievable submicrometer beam size. The traditional method for extracting elastic strain (and hence stress) and lattice orientation from a microdiffraction image relies on fitting each Laue spot with an analytical function to estimate the peak position on the detector screen. The method is thus limited to spots exhibiting ellipsoidal shapes, thereby impeding the study of specimens plastically deformed. To overcome this difficulty, the so-called Laue-DIC method introduces digital image correlation (DIC) for the evaluation of the relative positions of spots, which can thus be of any shape. This paper is dedicated to evaluating the accuracy of this Laue-DIC method. First, a simple image noise model is established and verified on the data acquired at beamline BM32 of the European Synchrotron Radiation Facility. Then, the effect of image noise on errors on spot displacement measured by DIC is evaluated by Monte Carlo simulation. Finally, the combined effect of the image noise, calibration errors and the number of Laue spots used for data treatment is investigated. Results in terms of the uncertainty of stress measurement are provided, and various error regimes are identified.
劳厄微衍射技术在多个同步辐射设施中均可实现,由于其可实现亚微米级的光束尺寸,非常适合用于测量变形材料中的晶内应力场。从微衍射图像中提取弹性应变(进而得到应力)和晶格取向的传统方法,是通过用解析函数拟合每个劳厄斑来估计探测器屏幕上的峰值位置。因此,该方法仅限于形状为椭圆形的斑点,从而阻碍了对塑性变形试样的研究。为克服这一困难,所谓的劳厄 - 数字图像相关(Laue-DIC)方法引入了数字图像相关技术来评估斑点的相对位置,这样斑点可以是任意形状。本文致力于评估这种劳厄 - DIC方法的准确性。首先,建立了一个简单的图像噪声模型,并在欧洲同步辐射设施的BM32光束线采集的数据上进行了验证。然后,通过蒙特卡罗模拟评估了图像噪声对DIC测量的斑点位移误差的影响。最后,研究了图像噪声、校准误差以及用于数据处理的劳厄斑数量的综合影响。给出了应力测量不确定度方面的结果,并确定了各种误差范围。