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具有增强抛光性能的核壳结构金刚石/针铁矿复合颗粒的合成

The Synthesis of the Core/Shell Structured Diamond/Akageneite Hybrid Particles with Enhanced Polishing Performance.

作者信息

Lu Jing, Xu Yongchao, Zhang Dayu, Xu Xipeng

机构信息

Institute of Manufacturing Engineering, Huaqiao University, Xiamen 361021, China.

MOE Engineering Research Center for Brittle Materials Machining, Huaqiao University, Xiamen 361021, China.

出版信息

Materials (Basel). 2017 Jun 20;10(6):673. doi: 10.3390/ma10060673.

Abstract

In this study, the synthesis of the core/shell structured diamond/akageneite hybrid particles was performed through one-step isothermal hydrolyzing. The hybrid particle was characterized by X-ray diffraction, field emission scanning electron microscopy, and Fourier transform infrared spectra. The test results overall reveal that the akageneite coating, phase β-FeO(OH), was uniformly coated onto the diamond surface. The polishing performance of the pristine diamond and hybrid particles for the sapphire substrate was evaluated respectively. The experimental results show that the hybrid particles exhibited improved polishing quality and prolonged effective processing time of polishing pad compared with diamond particles without compromising the material remove rate and surface roughness. The improved polishing behavior might be attributed to the β-FeOOH coating, which is conducive to less abrasive shedding and reducing the scratch depth.

摘要

在本研究中,通过一步等温水解法合成了核/壳结构的金刚石/针铁矿混合颗粒。采用X射线衍射、场发射扫描电子显微镜和傅里叶变换红外光谱对混合颗粒进行了表征。测试结果总体表明,β-FeO(OH)相的针铁矿涂层均匀地包覆在金刚石表面。分别评估了原始金刚石和混合颗粒对蓝宝石衬底的抛光性能。实验结果表明,与金刚石颗粒相比,混合颗粒在不影响材料去除率和表面粗糙度的情况下,具有更好的抛光质量和更长的抛光垫有效加工时间。抛光性能的改善可能归因于β-FeOOH涂层,它有利于减少磨粒脱落并降低划痕深度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/52c3/5554054/8cefc34435b4/materials-10-00673-g001.jpg

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