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一种使用玻璃焊料连接陶瓷与钛植入部件的新技术。

A Novel Technique for the Connection of Ceramic and Titanium Implant Components Using Glass Solder Bonding.

作者信息

Mick Enrico, Tinschert Joachim, Mitrovic Aurica, Bader Rainer

机构信息

Biomechanics and Implant Technology Research Lab, Department of Orthopaedics, University Medicine Rostock, Doberaner Strasse 142, Rostock 18057, Germany.

Praxis fuer Zahnheilkunde, Holzgraben 1-3, Aachen 52062, Germany.

出版信息

Materials (Basel). 2015 Jul 14;8(7):4287-4298. doi: 10.3390/ma8074287.

Abstract

Both titanium and ceramic materials provide specific advantages in dental implant technology. However, some problems, like hypersensitivity reactions, corrosion and mechanical failure, have been reported. Therefore, the combining of both materials to take advantage of their pros, while eliminating their respective cons, would be desirable. Hence, we introduced a new technique to bond titanium and ceramic materials by means of a silica-based glass ceramic solder. Cylindrical compound samples (Ø10 mm × 56 mm) made of alumina toughened zirconia (ATZ), as well as titanium grade 5, were bonded by glass solder on their end faces. As a control, a two-component adhesive glue was utilized. The samples were investigated without further treatment, after 30 and 90 days of storage in distilled water at room temperature, and after aging. All samples were subjected to quasi-static four-point-bending tests. We found that the glass solder bonding provided significantly higher bending strength than adhesive glue bonding. In contrast to the glued samples, the bending strength of the soldered samples remained unaltered by the storage and aging treatments. Scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) analyses confirmed the presence of a stable solder-ceramic interface. Therefore, the glass solder technique represents a promising method for optimizing dental and orthopedic implant bondings.

摘要

钛和陶瓷材料在牙种植技术中都具有特定优势。然而,已有报道称存在一些问题,如过敏反应、腐蚀和机械故障。因此,将两种材料结合起来以发挥其优点,同时消除各自的缺点,将是理想的。因此,我们引入了一种通过二氧化硅基玻璃陶瓷焊料来粘结钛和陶瓷材料的新技术。由氧化铝增韧氧化锆(ATZ)以及5级钛制成的圆柱形复合样品(Ø10毫米×56毫米)在其端面上通过玻璃焊料进行粘结。作为对照,使用了一种双组分粘合剂胶水。对样品在未经进一步处理、在室温下于蒸馏水中储存30天和90天后以及老化后进行了研究。所有样品均进行了准静态四点弯曲试验。我们发现,玻璃焊料粘结提供的弯曲强度明显高于粘合剂胶水粘结。与胶合样品不同,焊接样品的弯曲强度在储存和老化处理后保持不变。扫描电子显微镜(SEM)和能量色散X射线(EDX)分析证实了稳定的焊料 - 陶瓷界面的存在。因此,玻璃焊料技术是一种优化牙科和骨科植入物粘结的有前景的方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e1f1/5455666/39ed5570ca31/materials-08-04287-g001.jpg

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