Chen Ying, Ding Hao, Sun Sijia
Beijing Key Laboratory of Materials Utilization of Nonmetallic Minerals and Solid Wastes, National Laboratory of Mineral Materials, School of Materials Science and Technology, China University of Geosciences (Beijing), Beijing 100083, China.
Nanomaterials (Basel). 2017 Aug 10;7(8):217. doi: 10.3390/nano7080217.
In order to reduce the primary particle size of zinc oxide (ZnO) and eliminate the agglomeration phenomenon to form a monodisperse state, Zn was loaded on the surface of amorphous silica (SiO₂) by the hydrogen bond association between hydroxyl groups in the hydrothermal process. After calcining the precursors, dehydration condensation among hydroxyl groups occurred and ZnO nanoparticles supported on amorphous SiO₂ (ZnO-SiO₂) were prepared. Furthermore, the SEM and TEM observations showed that ZnO nanoparticles with a particle size of 3-8 nm were uniformly and dispersedly loaded on the surface of amorphous SiO₂. Compared with pure ZnO, ZnO-SiO₂ showed a much better antibacterial performance in the minimum inhibitory concentration (MIC) test and the antibacterial properties of the paint adding ZnO-SiO₂ composite.
为了减小氧化锌(ZnO)的一次粒径并消除团聚现象以形成单分散状态,在水热过程中通过羟基之间的氢键缔合将锌负载在无定形二氧化硅(SiO₂)表面。煅烧前驱体后,羟基之间发生脱水缩合,制备了负载在无定形SiO₂上的ZnO纳米颗粒(ZnO-SiO₂)。此外,扫描电子显微镜(SEM)和透射电子显微镜(TEM)观察表明,粒径为3-8nm的ZnO纳米颗粒均匀且分散地负载在无定形SiO₂表面。与纯ZnO相比,ZnO-SiO₂在最低抑菌浓度(MIC)测试以及添加ZnO-SiO₂复合材料的涂料的抗菌性能方面表现出更好的抗菌性能。