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激光 3D 打印制备 Ti6Al4V-V-Cr-Fe-SS316 多层金属结构的研究。

Investigation on Ti6Al4V-V-Cr-Fe-SS316 Multi-layers Metallic Structure Fabricated by Laser 3D Printing.

机构信息

Department of Mechanical and Aerospace Engineering, Missouri University of Science and Technology, Rolla, MO, 65409, United States.

Department of Metallurgical Engineering, Missouri University of Science and Technology, Rolla, MO, 65409, United States.

出版信息

Sci Rep. 2017 Aug 11;7(1):7977. doi: 10.1038/s41598-017-08580-z.

Abstract

Joining titanium alloy and stainless steel is becoming an urgent need since their outstanding mechanical properties can be utilized integratedly. However, direct fusion joining of Ti6Al4V to SS316 can cause brittle Ti-Fe intermetallics which compromise join bonds' mechanical properties. In this research, Laser 3D Printing was applied to explore a new Ti6Al4V to SS316 multi-metallic structure. A novel filler transition route was introduced (Ti6Al4V → V → Cr → Fe → SS316) to avoid the Ti-Fe intermetallics. Two experimental cases were performed for comparison to evaluate this novel route's effect. In the first case, SS316 layer was directly deposited on Ti6Al4V substrate by laser 3D printing, but the sample cracked in the printing process. Then fracture morphology, phase identification, and micro-hardness were analyzed. In the second case, a multi-metallic structure was fabricated via laser 3D printing following the transition route. Microstructure characterization and composition distribution were analyzed via scanning electron microscope(SEM) and energy dispersive spectrometry(EDS). x-ray diffraction(XRD) tests demonstrated the intermetallics were effectively avoided following the transition route. Vickers hardness number(VHN) showed no significant hard brittle phases in the sample. Comparing with directly depositing SS316 on Ti6Al4V, the usage of the novel transition route can eliminate the intermetallics effectively. These research results are good contributions in joining titanium alloy and stainless steel.

摘要

钛合金与不锈钢的连接成为一种迫切的需求,因为它们的优异机械性能可以得到综合利用。然而,钛 6 铝 4 钒与 SS316 的直接熔接会导致脆性的 Ti-Fe 金属间化合物,从而影响连接的机械性能。在这项研究中,激光 3D 打印被应用于探索一种新的钛 6 铝 4 钒与 SS316 的多金属结构。引入了一种新型的填充过渡路线(钛 6 铝 4 钒→钒→铬→铁→SS316)以避免 Ti-Fe 金属间化合物的形成。进行了两个实验案例进行比较,以评估这种新型路线的效果。在第一个案例中,通过激光 3D 打印直接在钛 6 铝 4 钒基底上沉积 SS316 层,但样品在打印过程中出现了裂纹。然后对其进行了断裂形貌、相鉴定和显微硬度分析。在第二个案例中,通过激光 3D 打印按照过渡路线制造了多金属结构。通过扫描电子显微镜(SEM)和能谱仪(EDS)分析了微观结构特征和成分分布。X 射线衍射(XRD)测试表明,按照过渡路线可以有效地避免金属间化合物的形成。维氏硬度数(VHN)表明样品中没有明显的硬脆相。与直接在钛 6 铝 4 钒上沉积 SS316 相比,新型过渡路线的使用可以有效地消除金属间化合物。这些研究结果为钛合金与不锈钢的连接做出了很好的贡献。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c0cc/5554222/287a79383eeb/41598_2017_8580_Fig1_HTML.jpg

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