Bociong Kinga, Szczesio Agata, Sokolowski Krzysztof, Domarecka Monika, Sokolowski Jerzy, Krasowski Michal, Lukomska-Szymanska Monika
University Laboratory of Materials Research, Medical University of Lodz, 251 Pomorska St., 92-213 Lodz, Poland.
Department of Restorative Dentistry, Medical University of Lodz, 251 Pomorska St., 92-213 Lodz, Poland.
Materials (Basel). 2017 Sep 28;10(10):1142. doi: 10.3390/ma10101142.
The contraction stress generated during the photopolymerization of resin dental composites is the major disadvantage. The water sorption in the oral environment should counteract the contraction stress. The purpose was to evaluate the influence of the water sorption of composite materials on polymerization shrinkage stress generated at the restoration-tooth interface. The following materials were tested: Filtek Ultimate, Gradia Direct LoFlo, Heliomolar Flow, Tetric EvoCeram, Tetric EvoCeram Bulk Fill, Tetric EvoFlow, Tetric EvoFlow Bulk Fill, X-tra Base, Venus BulkFil, and Ceram.X One. The shrinkage stress was measured immediately after curing and after: 0.5 h, 24 h, 72 h, 96 h, 168 h, 240 h, 336 h, 504 h, 672 h, and 1344 h by means of photoelastic study. Moreover, water sorption and solubility were evaluated. Material samples were weighted on scale in time intervals to measure the water absorbency and the dynamic of this process. The tested materials during polymerization generated shrinkage stresses ranging from 6.3 MPa to 12.5 MPa. Upon water conditioning (56 days), the decrease in shrinkage strain (not less than 48%) was observed. The decrease in value stress in time is material-dependent.
树脂牙科复合材料光聚合过程中产生的收缩应力是其主要缺点。口腔环境中的吸水作用应能抵消收缩应力。本研究旨在评估复合材料的吸水性能对修复体与牙齿界面处聚合收缩应力的影响。测试了以下材料:Filtek Ultimate、Gradia Direct LoFlo、Heliomolar Flow、Tetric EvoCeram、Tetric EvoCeram Bulk Fill、Tetric EvoFlow、Tetric EvoFlow Bulk Fill、X-tra Base、Venus BulkFil和Ceram.X One。通过光弹性研究在固化后以及0.5小时、24小时、72小时、96小时、168小时、240小时、336小时、504小时、672小时和1344小时后测量收缩应力。此外,还评估了吸水率和溶解性。通过定期对材料样本称重来测量吸水量及其过程动态。测试材料在聚合过程中产生的收缩应力范围为6.3MPa至12.5MPa。经过水调节(56天)后,观察到收缩应变降低(不低于48%)。应力值随时间的降低因材料而异。