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块状充填复合材料的收缩应力和弹性模量评估。

Shrinkage stress and elastic modulus assessment of bulk-fill composites.

机构信息

Case Western Reserve University, School of Dental Medicine, Department of Comprehensive Care, Cleveland, Ohio, USA.

University of São Paulo, Faculdade de Odontologia de Bauru, Departamento de Dentística, Endodontia e Materiais Odontológicos, Bauru, São Paulo, Brazil.

出版信息

J Appl Oral Sci. 2019 Jan 7;27:e20180132. doi: 10.1590/1678-7757-2018-0132.

Abstract

UNLABELLED

Bulk-fill composites were introduced in dentistry to accelerate clinical procedures while providing adequate outcomes. Concerns regarding the use of bigger composite increments rely on the polymerization shrinkage and shrinkage stress, which may generate gaps on the adhesive interface and result in a reduced success rate.

OBJECTIVE

To evaluate the polymerization shrinkage stress of different bulk-fill resin composites and their elastic modulus.

MATERIALS AND METHODS

Fourteen specimens were made for each of the nine different resin composites (seven with 12 mm3 and seven with 24 mm3): Surefill SDR flow (SDR), X-tra Base (XB), Filtek Bulk Fill Flowable (FBF), Filtek Z350XT Flow (Z3F); Tetric Evo Ceram Bulk Fill (TBF), X-tra Fil (XF), Filtek Bulk Fill (FBP), Admira Xtra Fusion (ADM) and Filtek Z350 XT (Z3XT). Linear shrinkage stress was evaluated for 300 s with the aid of a linear shrinkage device adapted to a Universal Testing Machine. For each composite group, seven additional specimens (2x2x25 mm) were made and Young's modulus was evaluated with a 3-point bending device adapted in a Universal Testing Machine with 0.5 mm/min crosshead speed and 50 KgF loading cell.

RESULTS

For 12 mm3 specimens, three-way ANOVA showed that only SDR and TBF generated lower stress after 20 s. Considering 300 s, TBF, SDR, and XF generated the lowest stress, followed by ADM, FBP, XB, and FBF, which were similar to Z3XT. Z3F generated the highest stress values for all time points. Considering 24 mm3 specimens after 20 s, all bulk fill composites generated lower stress than Z3XT, except XB. After 300 s, SDR, FBP, and ADM generated the lowest stress, followed by TBF and XF. For elastic modulus, one-way ANOVA showed that FBF, SDR, Z3F, and ADM presented the lowest values, followed by XB and TBF. FBP, Z3XT, and XF presented the highest elastic modulus among the evaluated composites.

CONCLUSIONS

Bulk-fill resin composites presented equal to lower shrinkage stress generation when compared to conventional composites, especially when bigger increments were evaluated. Bulk-fill composites showed a wide range of elastic modulus values, but usually similar to "regular" composites.

摘要

未加标签

为了加快临床操作速度,同时提供足够的效果,牙科领域引入了块状填充复合材料。对使用更大的复合材料增量的担忧依赖于聚合收缩和收缩应力,这可能会在粘合界面上产生间隙,并导致成功率降低。

目的

评估不同块状填充树脂复合材料的聚合收缩应力及其弹性模量。

材料和方法

对于九种不同的树脂复合材料(七种为 12mm³,七种为 24mm³),每种复合材料都制作了 14 个样本:Surefill SDR flow(SDR)、X-tra Base(XB)、Filtek Bulk Fill Flowable(FBF)、Filtek Z350XT Flow(Z3F);Tetric Evo Ceram Bulk Fill(TBF)、X-tra Fil(XF)、Filtek Bulk Fill(FBP)、Admira Xtra Fusion(ADM)和 Filtek Z350 XT(Z3XT)。借助于适用于万能试验机的线性收缩装置,在 300s 内评估线性收缩应力。对于每个复合材料组,另外制作了七个(2x2x25mm)样本,并使用适用于万能试验机的三点弯曲装置,以 0.5mm/min 的十字头速度和 50kgf 加载单元评估杨氏模量。

结果

对于 12mm³的样本,三因素方差分析表明,只有 SDR 和 TBF 在 20s 后产生的应力较低。考虑到 300s,TBF、SDR 和 XF 产生的应力最低,其次是 ADM、FBP、XB 和 FBF,与 Z3XT 相似。Z3F 在所有时间点产生的应力值最高。考虑到 20s 后的 24mm³样本,所有块状填充复合材料产生的应力均低于 Z3XT,除了 XB。在 300s 后,SDR、FBP 和 ADM 产生的应力最低,其次是 TBF 和 XF。对于弹性模量,单因素方差分析表明,FBF、SDR、Z3F 和 ADM 的值最低,其次是 XB 和 TBF。FBP、Z3XT 和 XF 在评估的复合材料中表现出最高的弹性模量。

结论

块状填充树脂复合材料在与传统复合材料相比时产生了相等或更低的收缩应力,特别是在评估更大的增量时。块状填充复合材料的弹性模量值范围较宽,但通常与“常规”复合材料相似。

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