Sutil Bruna Gabrielle da Silva, Susin Alexandre Henrique
Universidade Federal de Santa Maria, Programa de Pós-Graduação em Ciências Odontológicas, Santa Maria, RS, Brasil.
Universidade Federal de Santa Maria, Departamento de Odontologia Restauradora, Santa Maria, RS, Brasil.
J Appl Oral Sci. 2017 Sep-Oct;25(5):533-540. doi: 10.1590/1678-7757-2016-0500.
To evaluate the effects of dentin pretreatment and temperature on the bond strength of a universal adhesive system to dentin.
Ninety-six extracted non-carious human third molars were randomly divided into 12 groups (n=8) according to Scotchbond Universal Adhesive (SbU) applied in self-etch (SE) and etch-and-rinse (ER) mode, adhesive temperature (20°C or 37°C) and sodium bicarbonate or aluminum oxide air abrasion. After composite build up, bonded sticks with cross-sectional area of 1 mm2 were obtained to evaluate the microtensile bond strength (μTBS). The specimens were tested at a crosshead speed of 0.5 mm/min on a testing machine until failure. Fractured specimens were analyzed under stereomicroscope to determine the failure patterns in adhesive, cohesive (dentin or resin) and mixed fractures. The microtensile bond strength data was analyzed using two-way ANOVA and Tukey's test (α=5%).
Interaction between treatment and temperature was statistically significant for SbU applied in self-etch technique. Both dentin treatments showed higher bond strength for ER mode, regardless of adhesive temperature. When compared to control group, sodium bicarbonate increased bond strength of SbU in SE technique. Adhesive temperature did not significantly affect the μTBS of tested groups. Predominantly, adhesive failure was observed for all groups.
Dentin surface treatment with sodium bicarbonate air abrasion improves bond strength of SbU, irrespective of adhesive application mode, which makes this approach an alternative to increase adhesive performance of Scotchbond Universal Adhesive to dentin.
评估牙本质预处理和温度对通用粘结系统与牙本质粘结强度的影响。
96颗拔除的无龋人类第三磨牙根据3M Scotchbond Universal Adhesive(SbU)的应用模式(自酸蚀或酸蚀冲洗)、粘结温度(20°C或37°C)以及是否使用碳酸氢钠或氧化铝进行空气喷砂处理,随机分为12组(每组n = 8)。复合树脂充填后,制备横截面积为1mm²的粘结棒以评估微拉伸粘结强度(μTBS)。在试验机上以0.5mm/min的十字头速度对标本进行测试直至破坏。在立体显微镜下分析断裂的标本,以确定粘结、内聚(牙本质或树脂)和混合断裂的破坏模式。使用双向方差分析和Tukey检验(α = 5%)分析微拉伸粘结强度数据。
对于采用自酸蚀技术应用的SbU,处理和温度之间的相互作用具有统计学意义。无论粘结温度如何,两种牙本质处理在酸蚀冲洗模式下均显示出更高的粘结强度。与对照组相比,碳酸氢钠提高了自酸蚀技术中SbU的粘结强度。粘结温度对测试组的μTBS没有显著影响。所有组主要观察到粘结破坏。
用碳酸氢钠空气喷砂处理牙本质表面可提高SbU的粘结强度,无论粘结应用模式如何,这使得该方法成为提高3M Scotchbond Universal Adhesive与牙本质粘结性能的一种替代方法。