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胶束萃取在色谱测定法之前从水性样品中分离法莫替丁的应用。

Application of Micellar Extraction for Isolation of Famotidine from Aqueous Samples Prior to its Chromatographic Determination.

作者信息

Kiszkiel-Taudul Ilona, Starczewska Barbara, Karpińska Joanna, Kasabuła Monika

机构信息

Institute of Chemistry, University of Bialystok, 15-245 Białystok, Poland.

出版信息

J Surfactants Deterg. 2017;20(6):1401-1409. doi: 10.1007/s11743-017-2003-3. Epub 2017 Aug 12.

DOI:10.1007/s11743-017-2003-3
PMID:29200812
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5686284/
Abstract

Micellar extraction was applied to isolate famotidine from aqueous samples. This drug is an H receptor antagonist used for the treatment of stomach diseases. The process was performed with a mixture of anionic sodium dodecylsulfate and nonionic Triton X-114 surfactants. The effect of different parameters on the efficiency of the micellar extraction such as electrolyte and surfactant concentration, pH of sample, temperature, shaking and centrifugation time was investigated. The influence of foreign substances on a studied process was tested. The elaborated procedure was applied for HPLC-UV determination of famotidine in natural water samples. The calibration graph was recorded in the range 1.35-37.12 μg mL of the studied compound. The repeatability of the method was equal to 7.4%. The limit of detection and quantification values for the determination of famotidine by using the proposed method amounted to 0.40 and 1.25 μg mL, respectively.

摘要

采用胶束萃取法从水样中分离法莫替丁。这种药物是一种H受体拮抗剂，用于治疗胃部疾病。该过程使用阴离子十二烷基硫酸钠和非离子吐温X-114表面活性剂的混合物进行。研究了不同参数如电解质和表面活性剂浓度、样品pH值、温度、振荡和离心时间对胶束萃取效率的影响。测试了外来物质对所研究过程的影响。所阐述的方法用于天然水样中法莫替丁的高效液相色谱-紫外测定。在所研究化合物浓度为1.35 - 37.12 μg/mL范围内记录校准曲线。该方法的重复性为7.4%。采用所提出的方法测定法莫替丁的检测限和定量限分别为0.40和1.25 μg/mL。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/716639ece02c/11743_2017_2003_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/d9428afd3ffe/11743_2017_2003_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/e4ec6fbec7f6/11743_2017_2003_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/ad1e46c3c7b3/11743_2017_2003_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/eb243eeda015/11743_2017_2003_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/3c9f2592ad69/11743_2017_2003_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/18262d96cf47/11743_2017_2003_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/716639ece02c/11743_2017_2003_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/d9428afd3ffe/11743_2017_2003_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/e4ec6fbec7f6/11743_2017_2003_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/ad1e46c3c7b3/11743_2017_2003_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/eb243eeda015/11743_2017_2003_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/3c9f2592ad69/11743_2017_2003_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/18262d96cf47/11743_2017_2003_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ca48/5686284/716639ece02c/11743_2017_2003_Fig7_HTML.jpg

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