Płotka-Wasylka Justyna, Rutkowska Małgorzata, Cieślik Bartłomiej, Tyburcy Alan, Namieśnik Jacek
Department of Analytical Chemistry, Faculty of Chemistry, Gdańsk University of Technology, 11/12 Narutowicza Street, 80-233 Gdańsk, Poland.
J Anal Methods Chem. 2017;2017:5283917. doi: 10.1155/2017/5283917. Epub 2017 Oct 31.
The determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic properties of wine.
The study was focused on measuring the concentration levels of trace metals in fruit wines. Analysis of K, Ca, Fe, Zn, Cd, Mg, Pb, Sn, and Hg in so-called was carried out by AES, AAS, CV-AAS, and GF-AAS techniques. The calculated calibration curves showed good linearity range for all tested analytes (with coefficient of determination in the range from 0.989 to 0.999). The low values of the limit of detection (from 0.0031 g/L to 0.47 mg/L) and the limit of quantification (from 0.009 g/L to 1.41 mg/L) were obtained.
The allowed levels of metal in fruit wines are prescribed by the International Office for Grapes and Wines (OIV). The data obtained from the study area for all metals did not exceed the international limits.
由于多种原因,不同类型食品和饮料样品中金属的测定受到了广泛关注,其中最重要的原因是这些元素或其化合物的营养和毒性作用。葡萄酒/果酒中某些元素含量的知识尤为重要,因为过量摄入时它们具有毒性,而且它们似乎对葡萄酒的感官特性有影响。
该研究聚焦于测定果酒中痕量金属的浓度水平。通过原子发射光谱法(AES)、原子吸收光谱法(AAS)、冷蒸气原子吸收光谱法(CV-AAS)和石墨炉原子吸收光谱法(GF-AAS)对所谓的[此处原文缺失具体名称]中的钾、钙、铁、锌、镉、镁、铅、锡和汞进行了分析。计算得到的校准曲线对所有测试分析物均显示出良好的线性范围(测定系数在0.989至0.999之间)。获得了较低的检测限(从0.0031 g/L至0.47 mg/L)和定量限(从0.009 g/L至1.41 mg/L)。
国际葡萄与葡萄酒组织(OIV)规定了果酒中金属的允许含量水平。研究区域获得的数据显示所有金属含量均未超过国际限值。