Ton That Quang, Nguyen Thien Truong Van, Dang Huu Phuc, Le Hoan Ngoc, Vo Loan Kieu Thi, Nguyen Minh Huu Duc, Ngu Nhan Truong, Nguyen Thien S, Hansen Poul Erik
a Faculty of Chemistry , VNUHCM-University of Science , Ho Chi Minh City , Vietnam.
c Theoretical Physics Research Group , Ton Duc Thang University , Ho Chi Minh City , Vietnam.
Nat Prod Res. 2018 Nov;32(21):2529-2534. doi: 10.1080/14786419.2018.1425844. Epub 2018 Jan 24.
A new dehydrodigallic acid derivative (1), along with 19 known compounds, including 6 phenolic derivatives, 2 steroids and 11 triterpenoids were isolated from the ethanol extract of the root of Geum urbanum. Herein, there is the first report of steroid and triterpene in Geum urbanum. The purified metabolites were characterised by NMR spectroscopic and mass spectrometric analyses. The identification of the known compounds (2-20) was based on the comparison of their NMR spectroscopic features with previously published data. The structural characteristics of compound 1 were elucidated by comprehensive 1D and 2D NMR spectroscopic methods and acid hydrolysis.
从城水杨梅根的乙醇提取物中分离出一种新的脱氢没食子酸衍生物(1)以及19种已知化合物,包括6种酚类衍生物、2种甾体和11种三萜类化合物。本文首次报道了城水杨梅中的甾体和三萜类化合物。通过核磁共振光谱和质谱分析对纯化的代谢产物进行了表征。已知化合物(2 - 20)的鉴定是基于它们的核磁共振光谱特征与先前发表数据的比较。化合物1的结构特征通过综合的一维和二维核磁共振光谱方法以及酸水解得以阐明。