Fornaini Carlo, Poli Federica, Merigo Elisabetta, Brulat-Bouchard Nathalie, El Gamal Ahmed, Rocca Jean-Paul, Selleri Stefano, Cucinotta Annamaria
Department of Engineering and Architecture, University of Parma, Parco Area delle Scienze 181/A, 43124 Parma, Italy.
Micoralis Laboratory, Faculty of Dentistry, University of Cote d'Azur, 24 Avenue des Diables Bleus, 06357 Nice, France.
Bioengineering (Basel). 2018 Jan 31;5(1):10. doi: 10.3390/bioengineering5010010.
Lithium disilicate dental ceramic bonding, realized by using different resins, is strictly dependent on micro-mechanical retention and chemical adhesion. The aim of this in vitro study was to investigate the capability of a 1070 nm fiber laser for their surface treatment. Samples were irradiated by a pulsed fiber laser at 1070 nm with different parameters (peak power of 5, 7.5 and 10 kW, repetition rate (RR) 20 kHz, speed of 10 and 50 mm/s, and total energy density from 1.3 to 27 kW/cm²) and the thermal elevation during the experiment was recorded by a fiber Bragg grating (FBG) temperature sensor. Subsequently, the surface modifications were analyzed by optical microscope, scanning electron microscope (SEM), and energy dispersive X-ray spectroscopy (EDS). With a peak power of 5 kW, RR of 20 kHz, and speed of 50 mm/s, the microscopic observation of the irradiated surface showed increased roughness with small areas of melting and carbonization. EDS analysis revealed that, with these parameters, there are no evident differences between laser-processed samples and controls. Thermal elevation during laser irradiation ranged between 5 °C and 9 °C. A 1070 nm fiber laser can be considered as a good device to increase the adhesion of lithium disilicate ceramics when optimum parameters are considered.
通过使用不同的树脂实现的二硅酸锂牙科陶瓷粘结,严格依赖于微观机械固位和化学粘附。本体外研究的目的是研究1070 nm光纤激光器对其进行表面处理的能力。用1070 nm的脉冲光纤激光器以不同参数(峰值功率5、7.5和10 kW,重复频率(RR)20 kHz,速度10和50 mm/s,总能量密度1.3至27 kW/cm²)对样品进行辐照,并通过光纤布拉格光栅(FBG)温度传感器记录实验过程中的热升高情况。随后,通过光学显微镜、扫描电子显微镜(SEM)和能量色散X射线光谱(EDS)对表面改性进行分析。在峰值功率5 kW、RR 20 kHz和速度50 mm/s的条件下,对辐照表面的微观观察显示粗糙度增加,伴有小面积的熔化和碳化。EDS分析表明,在这些参数下,激光处理后的样品与对照之间没有明显差异。激光辐照期间的热升高范围在5℃至9℃之间。当考虑最佳参数时,1070 nm光纤激光器可被视为提高二硅酸锂陶瓷粘结力的良好设备。