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在含硅和镁离子的溶液中,等离子体电解氧化处理的Ti-6Al-4V合金上形成类骨磷灰石。

Bone-Like Apatite Formation on the Plasma Electrolytic Oxidation-Treated Ti-6Al-4V Alloy in Solution Containing Si and Mg Ions.

作者信息

Park Seon-Yeong, Choe D Han-Cheol

机构信息

Department of Dental Materials, Research Center of Nano-Interface Activation for Biomaterials, and Research Center for Oral Disease Regulation of the Aged, College of Dentistry, Chosun University, Gwangju, 61452, Korea.

出版信息

J Nanosci Nanotechnol. 2018 Feb 1;18(2):1439-1441. doi: 10.1166/jnn.2018.14879.

Abstract

The bon-like apatite formation on the plasma electrolytic oxidation (PEO)-treated Ti-6Al-4V alloy in solution containing Si and Mg ions was studied using various experimental techniques. A Ti-6Al-4V ELI disk and implant was used as a substrate for PEO. A pulsed DC power supply was used to apply a potential of 280 V in the electrolyte for 3 min. To examine the bioactivity, the PEO films formed implant specimens were immersed in a simulated body fluid (SBF) for 12 h. PEO-treated surface has large micro-pores and small micro-pores, and 5 Mg/Si and 20 Mg/Si coated surfaces showed the more small micro-pores than that of CaP coated surface. The peaks of the anatase and the hydroxyapatite phases after SBF immersion shifted to the left as compared to before SBF immersion. Numbers of cells increased, as Mg content increased on the PEO treated surface. Bone-like apatite is well formed on the Mg and Si contained surface.

摘要

使用各种实验技术研究了在含硅和镁离子的溶液中,经等离子体电解氧化(PEO)处理的Ti-6Al-4V合金上类骨磷灰石的形成。将Ti-6Al-4V ELI圆盘和植入物用作PEO的基底。使用脉冲直流电源在电解液中施加280 V的电势3分钟。为了检测生物活性,将形成PEO膜的植入标本浸入模拟体液(SBF)中12小时。PEO处理过的表面有大微孔和小微孔,5Mg/Si和20Mg/Si涂层表面比CaP涂层表面显示出更多的小微孔。与SBF浸泡前相比,SBF浸泡后锐钛矿相和羟基磷灰石相的峰向左移动。随着PEO处理表面上镁含量的增加,细胞数量增加。在含镁和硅的表面上形成了良好的类骨磷灰石。

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