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含Sr和Si离子电解液中微弧氧化Ti-6Al-4V合金的形貌变化

Morphology Changes of Plasma Electrolytic Oxidized Ti-6Al-4V Alloy in the Electrolytes Containing Sr and Si Ions.

作者信息

Yu Ji-Min, Choe Han-Cheol

机构信息

Department of Dental Materials and Research Center of Nano-Interface Activation for Biomaterials, College of Dentistry, Chosun University, 61452, Korea.

出版信息

J Nanosci Nanotechnol. 2018 Feb 1;18(2):1453-1456. doi: 10.1166/jnn.2018.14889.

Abstract

In this study, morphology changes of plasma electrolytic oxidized (PEO) Ti-6Al-4V alloy in the electrolytes containing Sr and Si ions were researched using field-emission scanning electron microscope, Image J program thin film X-ray diffraction, and energy dispersive X-ray spectroscopy. Pulsed DC power supplied Ti-6Al-4V alloy was used at a 280 V for 3 minutes in the electrolyte containing Sr and Si ions. To determine cell growth, human embryonic kidney cells 293 were grown at a density of 2 × 105 cells per 1.0 ml in well plates. The pore size decreased, as the content of Sr ion increased, whereas, the number of pores per area increased. The Ca/P ratio of PEO treated in electrolyte containing high Sr concentration showed the higher than those of in electrolyte containing low Sr concentration. The peak of HA is shifted to left side, as the concentration of Sr increased. Also, the number of cells increased, as the concentration of Sr increased.

摘要

在本研究中,使用场发射扫描电子显微镜、Image J程序薄膜X射线衍射和能量色散X射线光谱研究了在含Sr和Si离子的电解质中,等离子体电解氧化(PEO)Ti-6Al-4V合金的形态变化。在含Sr和Si离子的电解质中,以280 V的电压对脉冲直流电源供电的Ti-6Al-4V合金进行3分钟的处理。为了确定细胞生长情况,将人胚肾细胞293以每1.0 ml 2×105个细胞的密度接种在孔板中。随着Sr离子含量的增加,孔径减小,而单位面积的孔数增加。在高Sr浓度电解质中进行PEO处理的Ca/P比高于在低Sr浓度电解质中的Ca/P比。随着Sr浓度的增加,HA的峰向左移动。此外,随着Sr浓度的增加,细胞数量也增加。

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