Nam Hui-Gyun, Yu Seong Jun, Choi Hyeong Yeol, Jeong Young Gyu, Shin Kwanwoo, Choi Jae-Hak
J Nanosci Nanotechnol. 2018 Oct 1;18(10):7110-7114. doi: 10.1166/jnn.2018.15475.
In this study, pyrolyzed photoresist films (PPFs) were prepared using commercial SU8 photoresist by proton irradiation and pyrolysis. SU8 thin films were irradiated with high-energy proton ions and then pyrolyzed in a tube furnace at 1000 °C under inert atmosphere. The carbonization yield of the PPFs increased with an increasing fluence due to the formation of more crosslinked network structures at a higher fluence. The electrical resistance decreased with an increasing fluence due to the higher remaining thickness and carbonization yield at a higher fluence. Therefore, the PPFs prepared at 1 × 1016 ions/cm2 showed the maximum temperature of 150 °C at 20 V and a high electric power efficiency of 1.57 mW/°C.
在本研究中,通过质子辐照和热解,使用商用SU8光刻胶制备了热解光刻胶薄膜(PPFs)。SU8薄膜用高能质子离子辐照,然后在惰性气氛下于管式炉中在1000°C下热解。由于在较高注量下形成了更多交联网络结构,PPFs的碳化产率随注量增加而增加。由于在较高注量下剩余厚度和碳化产率更高,电阻随注量增加而降低。因此,在1×10¹⁶离子/cm²下制备的PPFs在20 V时显示出150°C的最高温度和1.57 mW/°C的高电功率效率。