United States Army, 36014 Wratten Loop, Ft. Hood, TX 76544, USA.
United States Air Force, 3650 Chambers Pass, Ft. Sam Houston, TX 78023, USA.
Dent Mater. 2018 Oct;34(10):1531-1541. doi: 10.1016/j.dental.2018.06.005. Epub 2018 Jun 28.
The purpose of this study was to investigate the effect of high-irradiance light-curing-units (LCUs) on the depth-of-cure (DoC) and degree-of-polymerization (DoP) of bulk-fill composites (BFCs).
The DoC of composites (Beautifil-Bulk, SHOFU; Filtek-Bulk-Fill, 3M ESPE; Tetric-EvoCeram-Bulk-Fill, Ivoclar; Sonic-Fill-2, Kerr; Venus-Bulk-Fill, Heraeus; Z250, 3M-ESPE) were measured according to ISO-4049 using high-irradiance LCUs (FlashMax-P3, CMS-Dental; SPEC3, Coltene) and conventional LCU (Paradigm, 3M-ESPE) for exposure times: 3/9-s, 3/20-s, and 10/20-s respectively. Using FTIR, the DoP per composite was measured at the bottom surface as a function of post-curing times for the LCUs at the same exposure times. Data was analyzed with nonlinear regression and ANOVA/Tukey.
Significant differences in DoC were found amongst the LCUs for the various exposure times. All BFCs failed to meet the DoC claimed by manufacturers and failed to satisfy ISO-4049 with the high-irradiance LCUs with 3-s exposures. Standard irradiance and 20-s exposures outperformed all other irradiance-exposure combinations for maximizing the DoC and DoP of BFCs. A minimum of 15.3J/cm radiant exposure was required to achieve an adequate maximum polymerization rate. Venus Bulk exhibited the highest DoC and DoP for any LCU-exposure-time combination.
Among the different combinations of BFCs and LCUs, DoC and DoP were always increased with longer exposure time, but there exists a theoretical radiant-exposure limit beyond which DoP or DoC remains unchanged. However, high DoC or DoP are not always associated with one another. Thus, the exposure-reciprocity law must be approached thoughtfully since irradiance and exposure can independently affect DoP and DoC.
本研究旨在探讨高辐照度光固化器(LCU)对大体积充填复合树脂(BFC)的固化深度(DOC)和聚合度(DP)的影响。
根据 ISO-4049 标准,使用高辐照度 LCU(FlashMax-P3,CMS-Dental;SPEC3,Coltene)和传统 LCU(Paradigm,3M-ESPE),分别在曝光时间为 3/9-s、3/20-s 和 10/20-s 下,测量 Beautifil-Bulk、SHOFU;Filtek-Bulk-Fill、3M ESPE;Tetric-EvoCeram-Bulk-Fill、Ivoclar;Sonic-Fill-2、Kerr;Venus-Bulk-Fill、Heraeus;Z250、3M-ESPE 等复合材料的 DOC。使用傅里叶变换红外光谱(FTIR),在相同的曝光时间下,针对各 LCU,在底部表面测量 DP 作为后固化时间的函数。采用非线性回归和方差分析/图基检验对数据进行分析。
不同曝光时间的 LCU 之间,DOC 存在显著差异。所有 BFC 均未达到制造商声称的 DOC,并且在使用高辐照度 LCU 进行 3-s 曝光时,未能满足 ISO-4049 的要求。标准辐照度和 20-s 曝光在最大程度提高 BFC 的 DOC 和 DP 方面优于所有其他辐照度-曝光组合。要实现足够高的聚合速率,需要至少 15.3J/cm 辐射能。在任何 LCU-曝光时间组合中,Venus Bulk 均表现出最高的 DOC 和 DP。
在不同的 BFC 和 LCU 组合中,随着曝光时间的延长,DOC 和 DP 始终增加,但存在一个理论的辐射暴露极限,超过该极限后,DP 或 DOC 保持不变。然而,高 DP 或 DOC 并不总是相互关联的。因此,必须慎重考虑曝光补偿定律,因为辐照度和曝光时间可以独立影响 DP 和 DOC。