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高强度固化灯对块状填充复合材料聚合的影响。

Effect of high-intensity curing lights on the polymerization of bulk-fill composites.

机构信息

United States Army, 36014 Wratten Loop, Ft. Hood, TX 76544, USA.

United States Air Force, 3650 Chambers Pass, Ft. Sam Houston, TX 78023, USA.

出版信息

Dent Mater. 2018 Oct;34(10):1531-1541. doi: 10.1016/j.dental.2018.06.005. Epub 2018 Jun 28.

Abstract

OBJECTIVES

The purpose of this study was to investigate the effect of high-irradiance light-curing-units (LCUs) on the depth-of-cure (DoC) and degree-of-polymerization (DoP) of bulk-fill composites (BFCs).

METHODS

The DoC of composites (Beautifil-Bulk, SHOFU; Filtek-Bulk-Fill, 3M ESPE; Tetric-EvoCeram-Bulk-Fill, Ivoclar; Sonic-Fill-2, Kerr; Venus-Bulk-Fill, Heraeus; Z250, 3M-ESPE) were measured according to ISO-4049 using high-irradiance LCUs (FlashMax-P3, CMS-Dental; SPEC3, Coltene) and conventional LCU (Paradigm, 3M-ESPE) for exposure times: 3/9-s, 3/20-s, and 10/20-s respectively. Using FTIR, the DoP per composite was measured at the bottom surface as a function of post-curing times for the LCUs at the same exposure times. Data was analyzed with nonlinear regression and ANOVA/Tukey.

RESULTS

Significant differences in DoC were found amongst the LCUs for the various exposure times. All BFCs failed to meet the DoC claimed by manufacturers and failed to satisfy ISO-4049 with the high-irradiance LCUs with 3-s exposures. Standard irradiance and 20-s exposures outperformed all other irradiance-exposure combinations for maximizing the DoC and DoP of BFCs. A minimum of 15.3J/cm radiant exposure was required to achieve an adequate maximum polymerization rate. Venus Bulk exhibited the highest DoC and DoP for any LCU-exposure-time combination.

SIGNIFICANCE

Among the different combinations of BFCs and LCUs, DoC and DoP were always increased with longer exposure time, but there exists a theoretical radiant-exposure limit beyond which DoP or DoC remains unchanged. However, high DoC or DoP are not always associated with one another. Thus, the exposure-reciprocity law must be approached thoughtfully since irradiance and exposure can independently affect DoP and DoC.

摘要

目的

本研究旨在探讨高辐照度光固化器(LCU)对大体积充填复合树脂(BFC)的固化深度(DOC)和聚合度(DP)的影响。

方法

根据 ISO-4049 标准,使用高辐照度 LCU(FlashMax-P3,CMS-Dental;SPEC3,Coltene)和传统 LCU(Paradigm,3M-ESPE),分别在曝光时间为 3/9-s、3/20-s 和 10/20-s 下,测量 Beautifil-Bulk、SHOFU;Filtek-Bulk-Fill、3M ESPE;Tetric-EvoCeram-Bulk-Fill、Ivoclar;Sonic-Fill-2、Kerr;Venus-Bulk-Fill、Heraeus;Z250、3M-ESPE 等复合材料的 DOC。使用傅里叶变换红外光谱(FTIR),在相同的曝光时间下,针对各 LCU,在底部表面测量 DP 作为后固化时间的函数。采用非线性回归和方差分析/图基检验对数据进行分析。

结果

不同曝光时间的 LCU 之间,DOC 存在显著差异。所有 BFC 均未达到制造商声称的 DOC,并且在使用高辐照度 LCU 进行 3-s 曝光时,未能满足 ISO-4049 的要求。标准辐照度和 20-s 曝光在最大程度提高 BFC 的 DOC 和 DP 方面优于所有其他辐照度-曝光组合。要实现足够高的聚合速率,需要至少 15.3J/cm 辐射能。在任何 LCU-曝光时间组合中,Venus Bulk 均表现出最高的 DOC 和 DP。

意义

在不同的 BFC 和 LCU 组合中,随着曝光时间的延长,DOC 和 DP 始终增加,但存在一个理论的辐射暴露极限,超过该极限后,DP 或 DOC 保持不变。然而,高 DP 或 DOC 并不总是相互关联的。因此,必须慎重考虑曝光补偿定律,因为辐照度和曝光时间可以独立影响 DP 和 DOC。

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