Liu Lei, Wu Yunxin, Gong Hai
Light Alloy Research Institute, Central South University, Changsha 410083, China.
State Key Laboratory of High Performance Complex Manufacturing, Central South University, Changsha 410083, China.
Materials (Basel). 2018 Aug 22;11(9):1496. doi: 10.3390/ma11091496.
To explore the effective way of grain refinement for 2219 aluminum alloy, the approach of 'thermal compression tests + solid solution treatment experiments' was applied to simulate the process of intermediate thermo-mechanical treatment. The effects of deformation parameters (i.e., temperature, strain, and strain rate) on microstructural evolution were also studied. The results show that the main softening mechanism of 2219 aluminum alloy during warm deformation process is dynamic recovery, during which the distribution of CuAl₂ phase changes and the substructure content increases. Moreover, the storage energy is found to be decreased with the increase in temperature and/or the decrease in strain rate. In addition, complete static recrystallization occurs and substructures almost disappear during the solid solution treatment process. The average grain size obtained decreases with the decrease in deforming temperature, the increase in strain rate, and/or the increase in strain. The grain refinement mechanism is related to the amount of storage energy and the distribution of precipitated particles in the whole process of intermediate thermal-mechanical treatment. The previously existing dispersed fine precipitates are all redissolved into the matrix, however, the remaining precipitates exist mainly by the form of polymerization.
为探索2219铝合金的有效细化途径,采用“热压缩试验+固溶处理实验”的方法模拟中间热机械处理过程。研究了变形参数(即温度、应变和应变速率)对微观组织演变的影响。结果表明,2219铝合金在温变形过程中的主要软化机制是动态回复,在此过程中CuAl₂相的分布发生变化,亚结构含量增加。此外,发现储能随温度升高和/或应变速率降低而降低。另外,在固溶处理过程中发生完全静态再结晶,亚结构几乎消失。获得的平均晶粒尺寸随变形温度降低、应变速率增加和/或应变增加而减小。晶粒细化机制与中间热机械处理全过程中的储能和析出相粒子分布有关。先前存在的弥散细小析出相全部重新溶解到基体中,然而,剩余的析出相主要以聚合形式存在。