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树脂基复合材料的动态和静态弯曲评估:ISO和微型弯曲试验的比较。

Dynamic and Static Flexural Appraisal of Resin-based Composites: Comparison of the ISO and Mini-flexural Tests.

作者信息

Yap A U, Eweis A H, Yahya N A

出版信息

Oper Dent. 2018 Sep/Oct;43(5):E223-E231. doi: 10.2341/17-224-L.

Abstract

The objective of this study was to determine the influence of specimen dimension and conditioning medium on the dynamic and static flexural properties of resin-based composites (RBCs). One conventional (Filtek Z350) and two bulk-fill RBCs (Filtek Bulk-fill and Beautifil-Bulk Restorative) were evaluated. Bar-shaped specimens with dimensions 25 × 2 × 2 mm (ISO flexural [IFT]) or 12 × 2 × 2 mm (mini-flexural [MFT]) were fabricated using customized stainless-steel molds, finished, measured, randomly divided into two groups, and conditioned in air or artificial saliva (SAGF) for seven days at 37°C. The specimens (n=10) were then subjected to dynamic and static three-point flexural testing. Data for storage modulus, loss modulus, loss tangent, flexural strength, and modulus were computed and subjected to t-test, analysis of variance/Tukey test, and Pearson correlation at a significance level of α = 0.05. For both IFT and MFT, significant differences in dynamic and static flexural properties were more prevalent between materials after storage in saliva. For both conditioning mediums, the strongest correlation between IFT and MFT was observed for flexural strength. While significant positive correlations were observed for all flexural properties with saliva, no significant correlations were detected for loss tangent and flexural modulus with air. For both IFT and MFT, storage in saliva appeared to be more discriminative than storage in air. As moderate to strong positive relationships exist between IFT and MFT for dynamic and static flexural properties, the mini-flexural test holds promise as a replacement for the ISO 4049 in view of its clinical relevance and greater efficiency.

摘要

本研究的目的是确定样本尺寸和调节介质对树脂基复合材料(RBC)动态和静态弯曲性能的影响。评估了一种传统的(Filtek Z350)和两种大块充填RBC(Filtek Bulk-fill和Beautifil-Bulk Restorative)。使用定制的不锈钢模具制作尺寸为25×2×2 mm(ISO弯曲[IFT])或12×2×2 mm(微型弯曲[MFT])的条形样本,进行精加工、测量,随机分为两组,并在37°C的空气中或人工唾液(SAGF)中调节7天。然后对样本(n = 10)进行动态和静态三点弯曲测试。计算储能模量、损耗模量、损耗角正切、弯曲强度和模量的数据,并进行t检验、方差分析/ Tukey检验以及显著性水平为α = 0.05的Pearson相关性分析。对于IFT和MFT,在唾液中储存后,材料之间动态和静态弯曲性能的显著差异更为普遍。对于两种调节介质,弯曲强度在IFT和MFT之间观察到最强的相关性。虽然所有弯曲性能与唾液之间均观察到显著的正相关,但损耗角正切和弯曲模量与空气之间未检测到显著相关性。对于IFT和MFT,在唾液中储存似乎比在空气中储存更具区分性。由于IFT和MFT在动态和静态弯曲性能方面存在中度至强的正相关关系,鉴于其临床相关性和更高的效率,微型弯曲测试有望替代ISO 4049。

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