Ping D H, Guo S Q, Imura M, Liu X, Ohmura T, Ohnuma M, Lu X, Abe T, Onodera H
National Institute for Materials Science, Sengen 1-2-1, Tsukuba, 305-0047, Japan.
Faculty of Engineering, Hokkaido University, Kita 13 Nishi8, Kita-ku, Sapporo, Hokkaido, 060-8628, Japan.
Sci Rep. 2018 Sep 24;8(1):14264. doi: 10.1038/s41598-018-32679-6.
Lath martensite is the dominant microstructural feature in quenched low-carbon Fe-C alloys. Its formation mechanism is not clear, despite extensive research. The microstructure of an Fe-0.05 C (wt.%) alloy water-quenched at various austenitizing temperatures has been investigated using transmission electron microscopy and a novel lath formation mechanism has been proposed. Body-centered cubic {112}〈111〉-type twin can be retained inside laths in the samples quenched at temperatures from 1050 °C to 1200 °C. The formation mechanism of laths with a twin substructure has been explained based on the twin structure as an initial product of martensitic transformation. A detailed detwinning mechanism in the auto-tempering process has also been discussed, because auto-tempering is inevitable during the quenching of low-carbon Fe-C alloys. The driving force for the detwinning is the instability of ω-Fe(C) particles, which are located only at the twinning boundary region. The twin boundary can move through the ω ↔ bcc transition in which the ω phase region represents the twin boundary.
板条马氏体是淬火低碳Fe-C合金中主要的微观结构特征。尽管进行了广泛研究,但其形成机制仍不清楚。利用透射电子显微镜研究了在不同奥氏体化温度下水淬的Fe-0.05 C(重量百分比)合金的微观结构,并提出了一种新的板条形成机制。在1050 °C至1200 °C温度下淬火的样品中,体心立方{112}〈111〉型孪晶可以保留在板条内部。基于孪晶结构作为马氏体转变的初始产物,解释了具有孪晶亚结构的板条的形成机制。还讨论了自回火过程中详细的去孪晶机制,因为在低碳Fe-C合金淬火过程中自回火是不可避免的。去孪晶的驱动力是仅位于孪晶边界区域的ω-Fe(C)颗粒的不稳定性。孪晶界可以通过ω ↔ bcc转变移动,其中ω相区域代表孪晶界。