Department of Cariology and Operative Dentistry, Department of Oral Health Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University.
Department of Advanced Biomaterials, Oral Health Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University.
Dent Mater J. 2019 Mar 31;38(2):233-240. doi: 10.4012/dmj.2018-044. Epub 2018 Nov 17.
The repair microshear bond strengths (µSBSs) to resin matrices in 4 different cured-composites after water storage (0, 60 s, 1 week, 1 month) were evaluated. Three different adhesive application methods to the cured-composites were performed; (1) none, (2) onestep self-etch adhesive application, and (3) one-step self-etch adhesive application with a silane coupling agent. Degree of conversion (DC) of the composite discs was determined using ATR/FT-IR with a time-based spectrum analysis. Initially, the amount of un-reacted resin monomers in the repaired cured-composite contributed to the bonding performance of newly-filled uncured-composite to resin matrix of the cured-composite. Adhesive application could not improve their repair µSBS. After 1-month of water-storage, the repair µSBS was dependent on material, which either reduced or did not and was not influenced by their amount of un-reacted resin monomers. When repairing aged composite resin, the appropriate adhesive application procedures were different among resin composites.
评估了水储存(0、60 秒、1 周、1 个月)后 4 种不同固化复合材料中修复微剪切粘结强度(µSBS)与树脂基质的关系。对固化复合材料进行了三种不同的粘结剂应用方法:(1)无处理,(2)一步自酸蚀粘结剂处理,(3)一步自酸蚀粘结剂处理后用硅烷偶联剂处理。使用基于时间的光谱分析的 ATR/FT-IR 确定复合盘的转化率(DC)。最初,修复固化复合材料中未反应的树脂单体的量有助于新填充的未固化复合材料与固化复合材料的树脂基质之间的粘结性能。粘结剂的应用并不能提高它们的修复µSBS。在水储存 1 个月后,修复µSBS 取决于材料,其要么减少,要么不减少,并且不受其未反应树脂单体的量的影响。在修复老化的复合材料树脂时,不同的树脂复合材料对合适的粘结剂应用程序的要求不同。