Department of Food Science and Technology, College of Agriculture, Isfahan University of Technology, Isfahan, 84156-83111, Iran.
Department of Food Science and Technology, College of Agriculture, Isfahan University of Technology, Isfahan, 84156-83111, Iran.
Int J Biol Macromol. 2019 Mar 1;124:946-954. doi: 10.1016/j.ijbiomac.2018.12.049. Epub 2018 Dec 3.
This research aimed to optimize the polysaccharides extraction of oleaster fruit and then to investigate the physicochemical and functional properties of extracted polysaccharides. Temperature, water to dry matter ratio, time, and alcohol ratio were considered as variables. Purity of extracted polysaccharides was considered as the response. Optimization of polysaccharides extraction from full grain oleaster showed that all variables had effects on the purity of extracted polysaccharides alone or by interacting with other variables. The results showed that the temperature, 60 °C; water to dry matter ratio, 53:1 (V/W); time, 5 h; and alcohol ratio of 2.9 (V/V) were the best conditions for achieving the highest purity in extracted polysaccharides. The extracted polysaccharides had the potential of emulsion formation with high stability; however, foamability was not observed in this polysaccharide. In addition, the solubility of polysaccharide powder was high, and it increased with an increase in temperature, which resulted in a decrease in water absorption indicating the effect of heat on the structure and the amount of water absorption of extracted polysaccharides. The results obtained from FTIR confirmed the polysaccharide nature of extracted powder, and the X-ray diffraction pattern of extracted polysaccharides showed its semi-crystalline structure.
本研究旨在优化沙枣果实多糖的提取工艺,并研究提取多糖的理化和功能特性。温度、料液比、时间和醇比对提取工艺条件进行优化。提取多糖的纯度作为响应值。全谷物沙枣多糖的提取优化表明,所有变量都单独或与其他变量相互作用影响提取多糖的纯度。结果表明,温度为 60°C,料液比为 53:1(V/W),时间为 5 h,醇比为 2.9(V/V),是获得最高纯度提取多糖的最佳条件。提取的多糖具有形成高稳定性乳液的潜力,但在该多糖中未观察到泡沫形成。此外,多糖粉末的溶解性高,并且随着温度的升高而增加,这导致吸水率降低,表明热对提取多糖的结构和吸水率有影响。FTIR 分析结果证实了提取粉末的多糖性质,提取多糖的 X 射线衍射图谱表明其具有半结晶结构。