Won Jong Woo, Park Chan Hee, Hong Jaekeun, Lee Chong Soo, Hong Seong-Gu
Metal Materials Division, Korea Institute of Materials Science, Changwon, 51508, Republic of Korea.
Graduate Institute of Ferrous Technology, Pohang University of Science and Technology, Pohang, 37673, Republic of Korea.
Sci Rep. 2019 Feb 14;9(1):2009. doi: 10.1038/s41598-019-38652-1.
The rolling texture formed in the conventional cold rolling process of commercially pure titanium (CP-Ti) for producing a metal sheet significantly limits the potential applications of CP-Ti sheets in various industrial sectors by impairing the formability. Here, we report that by exploiting a twinning-induced crystallographic texture modification, the rolling texture can be weakened and dispersed effectively, leading to a simultaneous improvement in the formability and yield strength. A two-stage cold rolling process was designed with intermediate annealing at a late stage of the conventional cold rolling process to generate deformation twins. The intermediate annealing drove the activation of [Formula: see text] twin and [Formula: see text] - [Formula: see text] double twin in the second stage of the rolling process by removing the internal reaction stress developed in the first stage of the rolling process through recrystallization, and the crystallographic feature of the [Formula: see text] twinned region, i.e., [Formula: see text] twin texture, was effective for type slips and [Formula: see text] twinning to accommodate a through-thickness strain as well as for reducing the planar anisotropy. This enhanced thinning capability and reduced planar anisotropy in the [Formula: see text] twin texture led to an improvement of the formability. We demonstrated the feasibility of the suggested two-stage cold rolling process with ASTM grade 2 CP-Ti.
在工业纯钛(CP-Ti)生产金属薄板的常规冷轧过程中形成的轧制织构,通过削弱可成形性,显著限制了CP-Ti薄板在各个工业领域的潜在应用。在此,我们报告,通过利用孪生诱导的晶体织构改性,可以有效地削弱和分散轧制织构,从而同时提高可成形性和屈服强度。设计了一种两阶段冷轧工艺,在常规冷轧工艺的后期进行中间退火以产生变形孪晶。中间退火通过再结晶消除轧制第一阶段产生的内应力,从而在轧制第二阶段驱动{10-12}孪晶和{10-12}-{11-21}双孪晶的激活,并且{10-12}孪晶区域的晶体学特征,即{10-12}孪晶织构,对于型滑移和{11-21}孪生有效,以适应全厚度应变并降低平面各向异性。这种在{10-12}孪晶织构中增强的变薄能力和降低平面各向异性导致可成形性的提高。我们用ASTM 2级CP-Ti证明了所建议的两阶段冷轧工艺的可行性。