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多种复杂形状的同步放电等离子烧结

Simultaneous Spark Plasma Sintering of Multiple Complex Shapes.

作者信息

Manière Charles, Torresani Elisa, Olevsky Eugene A

机构信息

Powder Technology Laboratory, Department of Mechanical Engineering, San Diego State University, San Diego, CA 92182, USA.

Department of NanoEngineering, University of California, San Diego, La Jolla, CA 92037, USA.

出版信息

Materials (Basel). 2019 Feb 13;12(4):557. doi: 10.3390/ma12040557.

Abstract

This work addresses the two great challenges of the spark plasma sintering (SPS) process: The sintering of complex shapes and the simultaneous production of multiple parts. A new controllable interface method is employed to concurrently consolidate two nickel gear shapes by SPS. A graphite deformable sub-mold is specifically designed for the mutual densification of both complex parts in a unique 40 mm powder deformation space. An energy efficient SPS configuration is developed to allow the sintering of a large-scale powder assembly under electric current lower than 900 A. The stability of the developed process is studied by electro-thermal-mechanical (ETM) simulation. The ETM simulation reveals that homogeneous densification conditions can be attained by inserting an alumina powder at the sample/punches interfaces, enabling the energy efficient heating and the thermal confinement of the nickel powder. Finally, the feasibility of the fabrication of the two near net shape gears with a very homogeneous microstructure is demonstrated.

摘要

这项工作解决了放电等离子烧结(SPS)工艺的两大挑战:复杂形状的烧结以及多个零件的同时生产。采用了一种新型可控界面方法,通过SPS同时固结两个镍齿轮形状。专门设计了一种石墨可变形子模具,用于在独特的40毫米粉末变形空间中使两个复杂零件相互致密化。开发了一种节能型SPS配置,以允许在低于900 A的电流下烧结大规模粉末组件。通过电热机械(ETM)模拟研究了所开发工艺的稳定性。ETM模拟表明,通过在样品/冲头界面插入氧化铝粉末,可以实现均匀的致密化条件,从而实现镍粉的高效加热和热约束。最后,证明了制造具有非常均匀微观结构的两个近净形齿轮的可行性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9a5a/6416649/1060ce75054a/materials-12-00557-g001.jpg

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