School of Engineering, Taylor's University, Lakeside Campus, No. 1, Jalan Taylor's, Subang Jaya, Selangor 47500, Malaysia.
Institute of Agricultural Engineering, Wrocław University of Environmental and Life Sciences, 37a Chełmońskiego Street, 51-630 Wrocław, Poland.
Molecules. 2019 Apr 24;24(8):1625. doi: 10.3390/molecules24081625.
The preservation of active constituents in through the removal of moisture is crucial in producing a final product with high antioxidant activity. This study aims to determine the influences of various drying methods and drying conditions on the antioxidant activity, volatiles and phytosterols content of . The drying methods used were convective drying (CD) at 40 °C, 50 °C and 60 °C; freeze drying; vacuum microwave drying (VMD) at 6, 9 and 12 W/g; and two-stage convective pre-drying followed by vacuum microwave finish drying (CPD-VMFD) at 50 °C and 9 W/g. The drying kinetics of are best described by the thin-layer model (modified Page model). The highest antioxidant activity, TPC and volatile concentration were achieved with CD at 40 °C. GC-MS analysis identified the presence of 51 volatiles, which were mostly present in all samples but with quantitative variation. The dominant volatiles in fresh are 2-hexenal (60.28 mg 100 g db), 1-hexanol (18.70 mg 100 g db) and salicylic acid (15.05 mg 100 g db). The concentration of phytosterols in fresh sample was 3647.48 mg 100 g db, and the major phytosterols present in fresh and dried samples were β-sitosterol (1162.24 mg 100 g db). CPD-VMFD was effective in ensuring the preservation of higher phytosterol content in comparison with CD at 50 °C. The final recommendation of a suitable drying method to dehydrate leaves is CD at 40 °C.
通过去除水分来保留 的活性成分对于生产具有高抗氧化活性的最终产品至关重要。本研究旨在确定各种干燥方法和干燥条件对 的抗氧化活性、挥发物和植物甾醇含量的影响。使用的干燥方法有:40°C、50°C 和 60°C 的对流干燥(CD);冷冻干燥;6、9 和 12 W/g 的真空微波干燥(VMD);以及 50°C 和 9 W/g 的两阶段对流预干燥 followed by vacuum microwave 完成干燥(CPD-VMFD)。 的干燥动力学最好用薄层模型(修正 Page 模型)来描述。在 40°C 的 CD 下,抗氧化活性、TPC 和挥发性浓度最高。GC-MS 分析鉴定出存在 51 种挥发性物质,这些物质在所有样品中都存在,但数量有所不同。新鲜 的主要挥发性物质为 2-己烯醛(60.28 mg 100 g db)、1-己醇(18.70 mg 100 g db)和水杨酸(15.05 mg 100 g db)。新鲜样品中植物甾醇的浓度为 3647.48 mg 100 g db,新鲜和干燥样品中主要的植物甾醇为 β-谷甾醇(1162.24 mg 100 g db)。与 50°C 的 CD 相比,CPD-VMFD 有效地确保了较高的植物甾醇含量的保留。将 叶片脱水的合适干燥方法的最终推荐是 40°C 的 CD。