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常规黏度大块充填树脂和传统复合树脂的形态化学特征、显微硬度、吸水性及溶解性

Morphochemical characterization, microhardness, water sorption, and solubility of regular viscosity bulk fill and traditional composite resins.

作者信息

Melo Rafaela A, Bispo Andressa de Souza Leite, Barbosa Gustavo A S, Galvão Marilia R, de Assunção Isauremi V, Souza Rodrigo O de Assunção, Borges Boniek C D

机构信息

Department of Dentistry, Federal University of Rio Grande do Norte (UFRN), Natal, Brazil.

出版信息

Microsc Res Tech. 2019 Sep;82(9):1500-1506. doi: 10.1002/jemt.23315. Epub 2019 Jun 14.

DOI:10.1002/jemt.23315
PMID:31199552
Abstract

OBJECTIVE

To evaluate the morphology of filler particles, chemical composition, microhardness (MH), water sorption (WSp), and solubility (WSl) of a regular viscosity bulk fill and traditional composite resins.

METHODS

Eighty samples (Ø:5 mm; height: 4 mm) were prepared according to the factors "composite" (Aura/SDI, FiltekZ250 XT/3M, Aura Bulk Fill/SDI, and Filtek Bulk Fill/3M) and "filling technique" (incremental and bulk) (n = 10). Vickers MH was measured on the top and bottom surfaces of each samples, and then WSp and WSl were obtained by means of mass gain and loss. Morphology of filler particles and chemical characteristics of composites were evaluated by scanning electron microscopy (SEM) and energy dispersity spectroscopy (EDS) in additional samples (n = 1/group). Data were analyzed using two- and three-way ANOVA and Tukey's tests (p < .05).

RESULTS

No significant difference was found for WSp among the groups. Comparing composites in the incremental technique, Aura bulk fill composite showed lower WSI than the other materials and in the bulk fill technique, Filtek Bulk Fill showed the lowest value. Filtek Bulk Fill showed higher MH than the other composites on the bottom surface when samples were produced by bulk filling.

CONCLUSION

The composites presented good physical properties, but the bulk fill ones showed better results for the bottom microhardness and solubility, although chemical elements and morphology were similar in general.

摘要

目的

评估常规粘度的大块充填复合树脂和传统复合树脂的填料颗粒形态、化学成分、显微硬度(MH)、吸水性(WSp)和溶解度(WSl)。

方法

根据“复合树脂”(奥罗拉/SDI、FiltekZ250 XT/3M、奥罗拉大块充填/SDI和Filtek大块充填/3M)和“充填技术”(分层充填和大块充填)因素制备80个样本(直径:5mm;高度:4mm)(n = 10)。在每个样本的顶面和底面测量维氏显微硬度,然后通过质量增加和减少获得吸水性和溶解度。在额外的样本(n = 1/组)中,通过扫描电子显微镜(SEM)和能谱仪(EDS)评估填料颗粒的形态和复合树脂的化学特性。使用双向和三向方差分析以及Tukey检验分析数据(p < 0.05)。

结果

各组间吸水性无显著差异。在分层充填技术中比较复合树脂时,奥罗拉大块充填复合树脂的溶解度低于其他材料;在大块充填技术中,Filtek大块充填的溶解度最低。当通过大块充填制备样本时,Filtek大块充填在底面的显微硬度高于其他复合树脂。

结论

复合树脂呈现出良好的物理性能,但大块充填复合树脂在底面显微硬度和溶解度方面表现更好,尽管总体上化学元素和形态相似。

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