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无帽流动型大块充填树脂复合材料的颜色稳定性、吸水性及溶解性评估

Evaluation of colour stability, water sorption and solubility of no-cap flowable bulk fill resin composites.

作者信息

Ömeroğlu Merve Kütük, Hekimoğlu Hüseyin Can

机构信息

Faculty of Dentistry, Department of Restorative Dentistry, Istanbul Okan University, Istanbul, Turkey.

Private Yenisehir Oral Healthcare Center, İstanbul, Turkey.

出版信息

BMC Oral Health. 2025 Apr 19;25(1):604. doi: 10.1186/s12903-025-05902-w.

Abstract

BACKGROUND

The aim of this study is to investigate the colour stability, water absorption, and solubility values of low viscosity bulk fill resin composites that do not require an additional layer in comparison with high viscosity and low viscosity bulk fill resin composites used as a base.

METHODS

In the present study, four different bulk fill resin composites were used: Charisma Bulk Flow One (Kulzer), Estelite Bulk Fill Flowable (Tokuyama), X-tra Base (VOCO), Filtek One Bulk Fill (3M ESPE). The resin composites were prepared as disc-shaped samples with a diameter of 5 mm and a thickness of 4 mm, then polymerized using a LED light device (Elipar DeepCureS, 3M ESPE). The samples were kept in artificial saliva and coffee solution for 28 days to determine water absorption, solubility levels and ∆E values, with measurements taken on days 7, 14, 21 and 28. Water absorption and solubility levels were calculated based on ISO4049:2009 specification, and mean colour change values were calculated based on CIEDE2000 formula. Repeated Measures ANOVA, along with post hoc Bonferroni, Tamhane, and Adjusted Bonferroni tests, were used for the statistical evaluation of the data (p < 0.05).

RESULTS

Among all composite groups at all time intervals, Charisma Bulk Flow One composite showed the highest water absorption, solubility, and discolouration values.

CONCLUSION

The water absorption, solubility and discolouration values of the resin composites used in this study were affected by the amount of filler in the resin structure. The clinical applicability of low-viscosity bulk-fill resin composites that do not require an additional capping layer should be carefully reassessed.

摘要

背景

本研究旨在调查与用作基底的高粘度和低粘度大体积充填树脂复合材料相比,无需额外分层的低粘度大体积充填树脂复合材料的颜色稳定性、吸水性和溶解度值。

方法

在本研究中,使用了四种不同的大体积充填树脂复合材料:Charisma Bulk Flow One(库尔泽)、Estelite Bulk Fill Flowable(德山)、X-tra Base(VOCO)、Filtek One Bulk Fill(3M ESPE)。将树脂复合材料制备成直径5毫米、厚度4毫米的圆盘形样品,然后使用LED光固化设备(Elipar DeepCureS,3M ESPE)进行聚合。将样品置于人工唾液和咖啡溶液中28天,以测定吸水性、溶解度水平和∆E值,分别在第7天、14天、21天和28天进行测量。根据ISO4049:2009规范计算吸水性和溶解度水平,并根据CIEDE2000公式计算平均颜色变化值。采用重复测量方差分析以及事后邦费罗尼检验、塔姆哈尼检验和调整后的邦费罗尼检验对数据进行统计学评估(p < 0.05)。

结果

在所有时间间隔的所有复合组中,Charisma Bulk Flow One复合材料的吸水性、溶解度和变色值最高。

结论

本研究中使用的树脂复合材料的吸水性、溶解度和变色值受树脂结构中填料量的影响。对于无需额外覆盖层的低粘度大体积充填树脂复合材料的临床适用性,应谨慎重新评估。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bd6f/12009527/0dfbcbedfc2d/12903_2025_5902_Fig1_HTML.jpg

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