Duman Ayse Nurcan, Dogan Arife
Department of Prosthodontics, Faculty of Dentistry, Gazi University, 06490 Ankara, Türkiye.
Polymers (Basel). 2025 Mar 14;17(6):774. doi: 10.3390/polym17060774.
The aim of this in vitro study is to evaluate the effect of resin type and placement technique on the hardness of resin-based composites (RBCs). A total of 300 samples consisting of five RBCs (Filtek Z250 microhybrid, Filtek P60 packable, Tetric Ceram hybrid, Admira ORMOCER, and Tetric Flow flowable RBCs) were prepared. Each RBC was placed into Teflon molds with a 4 mm diameter and 2 or 8 mm depths with standard, bulk and incremental techniques and was polymerized by second-generation LED (Hilux Ledmax 1055, 229.153 mW/cm) and UV (ELC-410, 26.106 mW/cm) light-curing units (LCUs) in standard mode (n = 10). The Vickers hardness number (VHN) was measured from the top and bottom surfaces of the RBCs. Data were statistically analyzed with a one-way ANOVA. Multiple comparisons were made using the Tukey, Scheffe, and -tests ( < 0.05). The VHN of the RBCs polymerized with LED and UV LCUs varied between 110.33 and 25.16 and between 104.86 and 34.20, respectively. The Tetric Flow RBC did not polymerize with the LCUs on either surface. The RBCs placed using the bulk technique could not polymerize with the UV LCU on the top surface, except for the Filtek P60 RBC, but showed a higher VHN on the bottom surface. These significant findings highlight that the hardness is specific to the RBC material and placement technique.
本体外研究的目的是评估树脂类型和放置技术对树脂基复合材料(RBC)硬度的影响。共制备了300个样本,由五种RBC(Filtek Z250微混合树脂、Filtek P60可压实树脂、Tetric Ceram混合树脂、Admira ORMOCER树脂和Tetric Flow流动树脂基复合材料)组成。每种RBC采用标准、整体和增量技术放入直径4 mm、深度2或8 mm的聚四氟乙烯模具中,并通过第二代LED(Hilux Ledmax 1055,229.153 mW/cm)和UV(ELC - 410,26.106 mW/cm)光固化单元(LCU)以标准模式进行聚合(n = 10)。从RBC的顶面和底面测量维氏硬度值(VHN)。数据采用单因素方差分析进行统计学分析。使用Tukey、Scheffe和t检验进行多重比较(P < 0.05)。用LED和UV LCU聚合的RBC的VHN分别在110.33至25.16和104.86至34.20之间变化。Tetric Flow RBC在两个表面上均未与LCU聚合。采用整体技术放置的RBC,除Filtek P60 RBC外,顶面无法与UV LCU聚合,但底面显示出较高的VHN。这些重要发现突出表明,硬度因RBC材料和放置技术而异。