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激光超声无损评估颗粒增强金属基复合材料中的孔隙率。

Laser-ultrasonic nondestructive evaluation of porosity in particulate reinforced metal-matrix composites.

机构信息

Faculty of Physics, M.V. Lomonosov Moscow State University, Leninskie Gory, Moscow 119991, Russia.

A.A. Baikov Institute of Metallurgy and Material Science of Russian Academy of Sciences, Leninskii Prospect 49, Moscow 119991, Russia.

出版信息

Ultrasonics. 2019 Nov;99:105959. doi: 10.1016/j.ultras.2019.105959. Epub 2019 Jul 5.

Abstract

In this work, we propose the laser-ultrasonic method for nondestructive evaluation of porosity in particulate reinforced metal-matrix composites fabricated by stir and in-situ reactive casting techniques. The method is based on the influence of porosity on dispersion of the phase velocity of longitudinal acoustic waves, which is measured by the broadband acoustic spectroscopy with laser excitation of ultrasound (laser-ultrasonic spectroscopy). We studied stir cast hypereutectic aluminum-silicon alloy A336 matrix composites reinforced with the SiC micro particles (3.3-13.5 vol%) and in-situ reactive cast Al/AlTi composites reinforced with the AlTi intermetallic particles (4-11.5 vol%). In the spectral range of 3-40 MHz, the phase-velocity dispersion in both types of composites was observed: the high-frequency velocity in the range of 20-40 MHz increases with the increase of the reinforcement content independent of porosity, whereas the low-frequency velocity in the range of 3-10 MHz decreases with the increase of porosity independent of the reinforcement content. As a result, the relative dispersion grows up with the increase in the composite porosity independent of the variation in the reinforcement content. The empirical dependence between the porosity in a scanning composite region and the relative phase-velocity dispersion in this region is approximated by the same unified function. For the first time, such unified porosity-phase velocity functional relationship is obtained for particulate reinforced metal-matrix composites completely different in fabrication techniques as well as in chemical composition and elastic properties of reinforcing particles.

摘要

在这项工作中,我们提出了激光超声法用于评估搅拌和原位反应铸造技术制备的颗粒增强金属基复合材料中的孔隙率。该方法基于孔隙率对纵向声速相速度分散的影响,通过宽带声学光谱法和激光超声激发(激光超声光谱法)来测量。我们研究了搅拌铸造过共晶铝硅合金 A336 基体复合材料,该复合材料增强了 SiC 微颗粒(3.3-13.5vol%),以及原位反应铸造的 Al/AlTi 复合材料,该复合材料增强了 AlTi 金属间化合物颗粒(4-11.5vol%)。在 3-40MHz 的光谱范围内,观察到了这两种类型的复合材料中的相速度色散:20-40MHz 范围内的高频速度随着增强体含量的增加而增加,与孔隙率无关,而 3-10MHz 范围内的低频速度随着孔隙率的增加而减小,与增强体含量无关。因此,复合材料孔隙率的增加会导致相对相速度分散的增加,而与增强体含量的变化无关。扫描复合材料区域中的孔隙率与该区域中相对相速度分散之间的经验关系通过相同的统一函数进行近似。这是首次获得用于颗粒增强金属基复合材料的统一的孔隙率-相速度功能关系,这些复合材料在制造技术、增强颗粒的化学成分和弹性性能方面完全不同。

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