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采用响应面法,以菠萝蜜不可食用部分合成的纤维素纳米颗粒增强包装膜的制备。

Fabrication of packaging film reinforced with cellulose nanoparticles synthesised from jack fruit non-edible part using response surface methodology.

机构信息

Department of Food Process Engineering, School of Bioengineering, SRM Institute of Science and Technology, Kattankulathur, Tamil Nadu 603203, India.

Department of Food Process Engineering, School of Bioengineering, SRM Institute of Science and Technology, Kattankulathur, Tamil Nadu 603203, India.

出版信息

Int J Biol Macromol. 2020 Jan 1;142:63-72. doi: 10.1016/j.ijbiomac.2019.09.066. Epub 2019 Sep 12.

Abstract

In this study, a bionanocomposite based food packaging film was designed to reduce environmental hazards. Cellulose nanoparticles (CNP) were prepared from the non-edible part of jackfruit (Artocarpus heterophyllus) by alkaline treatment, bleaching, and acid hydrolysis. The newly designed bionanocomposite film consists of CNP, polyvinyl alcohol (PVA) and fennel seed essential oil (EO). The composition of the film was optimized using central composite design of response surface methodology. Quadratic models were developed for responses such as elongation at break, tensile strength, free radical scavenging (antioxidant) activity, and antimicrobial activity. The optimized film reported seven-fold increase in tensile strength and six-fold in elongation at break compared to PVA film due to incorporation of CNP. Quality of the optimized film was further confirmed by evaluating morphological features, surface characteristics, physical and thermal properties. The results suggest that the newly designed EO incorporated CNP-PVA bionanocomposite film as a better alternative for traditional food packaging materials.

摘要

在这项研究中,设计了一种基于生物纳米复合材料的食品包装薄膜,以减少对环境的危害。通过碱性处理、漂白和酸水解,从不可食用的菠萝蜜(Artocarpus heterophyllus)部分制备出纤维素纳米颗粒(CNP)。新设计的生物纳米复合材料薄膜由 CNP、聚乙烯醇(PVA)和茴香籽油(EO)组成。使用响应面法的中心复合设计优化了薄膜的组成。针对断裂伸长率、拉伸强度、自由基清除(抗氧化)活性和抗菌活性等响应,开发了二次模型。与 PVA 薄膜相比,由于加入了 CNP,优化后的薄膜的拉伸强度提高了七倍,断裂伸长率提高了六倍。通过评估形态特征、表面特性、物理和热性能,进一步证实了优化后的薄膜的质量。结果表明,新设计的含有 EO 的 CNP-PVA 生物纳米复合材料薄膜是传统食品包装材料的更好替代品。

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