Department of Physics, University of Wuppertal, Gaußstraße 20, 40227 Wuppertal, Germany.
Institute of High Energy Physics, Yuquan Road 19B, Beijing 100049, People's Republic of China.
J Synchrotron Radiat. 2019 Nov 1;26(Pt 6):1879-1886. doi: 10.1107/S1600577519011123. Epub 2019 Oct 16.
X-ray double-crystal monochromators face a shift of the exit beam when the Bragg angle and thus the transmitted photon energy changes. This can be compensated for by moving one or both crystals accordingly. In the case of monolithic channel-cut crystals, which exhibit utmost stability, the shift of the monochromated beam is inevitable. Here we report performance tests of novel, asymmetrically cut, channel-cut crystals which reduce the beam movements by more than a factor of 20 relative to the symmetric case over the typical energy range of an EXAFS spectrum at the Cu K-edge. In addition, the presented formulas for the beam offset including the asymmetry angle directly indicate the importance of this value, which has been commonly neglected so far in the operation of double-crystal monochromators.
X 射线双晶单色器在布拉格角变化时,出射光束会发生偏移,从而导致透射光子能量发生变化。这可以通过相应地移动一个或两个晶体来补偿。在具有最大稳定性的整体式通道切割晶体的情况下,单色化光束的偏移是不可避免的。在这里,我们报告了新型非对称切割通道切割晶体的性能测试结果,与对称情况相比,在 Cu K 边缘的典型 EXAFS 光谱能量范围内,该晶体将光束移动减少了 20 多倍。此外,给出的包括非对称角度在内的光束偏移公式直接表明了该值的重要性,迄今为止,在双晶单色器的操作中,该值通常被忽略。