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一种使用高压脉冲气相(HVPG)技术合成银、银/锗、银/二氧化钛、氧化锡和银/氧化锡纳米材料的标准方法。

A standard method to synthesize Ag, Ag/Ge, Ag/TiO, SnO, and Ag/SnO nanomaterials using the HVPG technique.

作者信息

Muflikhun Muhammad Akhsin, Santos Gil Nonato C

机构信息

Department of Mechanical and Industrial Engineering, Faculty of Engineering, Gadjah Mada University, Jl. Grafika No.2, Yogyakarta 55281, Indonesia.

Physics Department, De La Salle University, 2401 Taft Avenue, Manila, Philippines.

出版信息

MethodsX. 2019 Nov 28;6:2861-2872. doi: 10.1016/j.mex.2019.11.025. eCollection 2019.

Abstract

Nanotechnology is growing rapidly in the past few decades with the applications in several fields such as medicine, environment, energy, electronics, automotive, and aerospace. There are many methods used by researchers to synthesize nanomaterial. In this paper, Horizontal Vapor Phase Growth (HVPG) technique was successfully used to synthesize various nanomaterial and nanocomposite materials such as Ag, Ag/Ge, Ag/TiO, SnO, and Ag/SnO. HVPG technique used a one-pot step to synthesize nanomaterials with 100 % purity of the results, affordable cost, and environmentally friendly. The method has two variables; growth temperature and curing time. Changing the variables create different shapes of nanomaterials. It also reported that the technique could be used to synthesize various nanomaterials consists of single or multi-material. This detailed method demonstrates the capability of the HVPG technique to synthesize nanomaterials, not only to grow the single shape of nanomaterials but also allow other nanomaterial shapes to grow in different parameter conditions. •HVPG technique successfully used to synthesize various nanomaterials.•Only 2 parameters used; curing time and growth temperature.•Purity result (100 %) with no pollutant.

摘要

在过去几十年中,纳米技术发展迅速,并在医学、环境、能源、电子、汽车和航空航天等多个领域得到应用。研究人员使用了多种方法来合成纳米材料。在本文中,水平气相生长(HVPG)技术成功用于合成各种纳米材料和纳米复合材料,如银、银/锗、银/二氧化钛、氧化锡和银/氧化锡。HVPG技术采用一锅法步骤来合成纳米材料,所得产物纯度为100%,成本低廉且环保。该方法有两个变量:生长温度和固化时间。改变这些变量会产生不同形状的纳米材料。还报道称,该技术可用于合成由单一材料或多种材料组成的各种纳米材料。这种详细的方法展示了HVPG技术合成纳米材料的能力,不仅能生长单一形状的纳米材料,还能在不同参数条件下使其他形状的纳米材料生长。

•HVPG技术成功用于合成各种纳米材料。

•仅使用两个参数;固化时间和生长温度。

•产物纯度为(100%)且无污染物。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/29bb/6909336/01aa65220948/fx1.jpg

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