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通过原位生长硼酸铝晶须实现氧化铝与蓝宝石的连接以及晶须与蓝宝石衬底的取向关系。

Joining Alumina and Sapphire by Growing Aluminium Borate Whiskers In-Situ, and the Whiskers' Orientation Relationship with the Sapphire Substrate.

作者信息

Li Chun, Si Xiaoqing, Wu Shuang, Qi Junlei, Huang Yongxian, Feng Jicai, Cao Jian

机构信息

State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001, China.

出版信息

Materials (Basel). 2020 Jan 1;13(1):175. doi: 10.3390/ma13010175.

Abstract

Bonding between polycrystal alumina and sapphire with (0001), (10 1 ¯ 0), (11 2 ¯ 0), (1 1 ¯ 02) orientations is successfully achieved by growing aluminium borate whiskers in the joint. The morphology of the whiskers in the joint is characterised by (Scanning Electron Microscopy) SEM. The relationship between the growing direction of the aluminium borate whiskers and the orientation of the sapphire substrate is investigated. The effect of the growing direction of the aluminium borate whiskers on the mechanical properties of the joint is discussed. The results show that the whiskers on the sapphire with (10 1 ¯ 0) orientation grow perpendicular to the surface of the substrate while the whiskers show a random growth on the other substrates. It is found that there is an orientation relationship between the whiskers (220) and sapphire (10 1 ¯ 0) and the morphology of the whiskers has great influence on the mechanical properties of the joint. The joint between polycrystal alumina and sapphire with (10 1 ¯ 0) orientation exhibits the highest strength, which reaches 26 MPa.

摘要

通过在接头处生长硼酸铝晶须,成功实现了多晶氧化铝与具有(0001)、(10 1 ¯ 0)、(11 2 ¯ 0)、(1 1 ¯ 02)取向的蓝宝石之间的键合。接头处晶须的形态通过扫描电子显微镜(SEM)进行表征。研究了硼酸铝晶须的生长方向与蓝宝石衬底取向之间的关系。讨论了硼酸铝晶须的生长方向对接头力学性能的影响。结果表明,具有(10 1 ¯ 0)取向的蓝宝石上的晶须垂直于衬底表面生长,而在其他衬底上晶须呈随机生长。发现晶须(220)与蓝宝石(10 1 ¯ 0)之间存在取向关系,且晶须的形态对接头的力学性能有很大影响。多晶氧化铝与具有(10 1 ¯ 0)取向的蓝宝石之间的接头表现出最高强度,达到26MPa。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fe60/6981370/e4c6a897637a/materials-13-00175-g001.jpg

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