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添加纳米银对颌面硅橡胶弹性体材料物理机械性能的影响——一项体外研究。

Effect of adding silver nanoparticle on physical and mechanical properties of maxillofacial silicone elastomer material-an in-vitro study.

机构信息

Department of Prosthodontics Crown and Bridge and Implantology, Rajarajeswari Dental College and Hospital, No.14, Ramohalli Cross, Kumbalgodu, Mysore Road, Bangalore 560074, India.

Department of Prosthodontics, Rajarajeswari Dental College and Hospital, Bangalore, India.

出版信息

J Prosthodont Res. 2020 Oct;64(4):431-435. doi: 10.1016/j.jpor.2019.12.001. Epub 2020 Feb 13.

DOI:10.1016/j.jpor.2019.12.001
PMID:32063540
Abstract

PURPOSE

The purpose of this study was to evaluate the impact of silver nanoparticle incorporation into maxillofacial silicone material on its hardness, tear strength and color stability.

METHODS

A total of 180 silicone specimens were fabricated according to the specification of American society for material and testing (ASTM) No. D142 and No. D624. The control samples were fabricated without silver nanoparticles and test samples were fabricate with 20 ppm concentration of silver nanoparticles. For outdoor weathering specimens were placed in a metal cage, which was suspended from the roof for a period of one month. Digital shore A hardness tests (Yuzuki, DIN 53505, ASTM D2240) was used to measure hardness, for tear strength the specimen was placed in the jaws of the universal testing machine (Lloyd instruments, LR 50 K) and stretched at a rate of 500 ram/rain, for color stability Spectrophotometer had been employed and the data recorded in the CIE Lab* system. The independent sample's "t" test was used to test significant differences.

RESULTS

The mean difference for hardness between control and test group was 0.54 and t value was 2.08 and (p < 0.05).tear strength 0.66 and "t" value was 0.93 and (p < 0.05) and for color stability it was -0.02 and t value was -0.92 and (p < 0.05).

CONCLUSION

The present study findings suggest that addition of silver nanoparticles at 20 ppm concentration decreased the hardness of Teksil 25(S25) silicone elastomer, and it did not affect tear strength and color stability.

摘要

目的

本研究旨在评估将纳米银颗粒掺入颌面硅橡胶材料对其硬度、撕裂强度和颜色稳定性的影响。

方法

根据美国材料与试验协会(ASTM)标准 No.D142 和 No.D624 制作了 180 个硅橡胶样本。对照组样本未添加纳米银颗粒,实验组样本则添加了 20ppm 浓度的纳米银颗粒。户外耐候性测试样本被放置在金属笼中,悬挂在屋顶下一个月。使用数位邵氏硬度计(Yuzuki,DIN 53505,ASTM D2240)测量硬度,使用万能试验机(Lloyd 仪器,LR 50K)的夹具夹持试样,以 500ram/min 的速率拉伸,测量撕裂强度,使用分光光度计以 CIE Lab*系统记录颜色稳定性数据。采用独立样本“t”检验来检验显著性差异。

结果

硬度方面,对照组和实验组的平均差值为 0.54,t 值为 2.08,(p<0.05)。撕裂强度的差值为 0.66,t 值为 0.93,(p<0.05),颜色稳定性的差值为-0.02,t 值为-0.92,(p<0.05)。

结论

本研究结果表明,在 20ppm 浓度下添加纳米银颗粒会降低 Teksil 25(S25)硅橡胶弹性体的硬度,但不会影响撕裂强度和颜色稳定性。

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