Tie Di, Wang Yu, Wang Xiang, Guan Renguo, Yan Lufei, Zhang Jin, Cai Zhihui, Zhao Yang, Gao Fei, Liu Haifeng
Key Laboratory of Lightweight Structural Materials Liaoning Province, School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China.
School of Materials Science and Engineering, Northwestern Polytechnical University, Xi'an 710072, China.
Materials (Basel). 2020 Feb 13;13(4):845. doi: 10.3390/ma13040845.
Low-cost heat-resistant Al-Sc-Zr-Fe conductor wires were successfully manufactured by continuous rheo-extrusion process, and the mechanical and conductive properties of the materials were analyzed and compared after three different thermo-mechanical treatment methods. The coarse plate-shape AlFe phase transformed to small sized rod-like phase after solid solution treatment at 630 °C for 21 h. Direct aging treatment at 300 °C for 24 h led to the refinement and spheroidization of AlFe phase with a diameter of 200 nm. After the subsequent aging treatment at 300 °C for 24 h, the tensile strength and conductivity of the alloy wire significantly increased due to the homogeneous precipitation of the coherent spherical Al(Sc, Zr) phase with an average size of 15 nm. The tensile strength, elongation, and conductivity of the alloy conductor wire after optimized thermo-mechanical treatment reached 165.7 MPa, 7.3%, and 60.26% International Annealed Copper Standard (IACS), respectively. The thermal resistance of the present alloy wire was superior to that of standard AT1 type alloy conductor according to IEC international standard.
采用连续流变挤压工艺成功制备了低成本耐热Al-Sc-Zr-Fe导线,并对材料在三种不同热机械处理方法后的力学性能和导电性能进行了分析和比较。在630℃固溶处理21 h后,粗大的板状AlFe相转变为细小的棒状相。在300℃直接时效处理24 h导致AlFe相细化并球化,直径为200 nm。在随后300℃时效处理24 h后,由于平均尺寸为15 nm的相干球形Al(Sc, Zr)相的均匀析出,合金丝的抗拉强度和电导率显著提高。经过优化热机械处理后的合金导线的抗拉强度、伸长率和电导率分别达到165.7 MPa、7.3%和60.26%国际退火铜标准(IACS)。根据IEC国际标准,本合金丝的热阻优于标准AT1型合金导体。