Wang Jiahui, Liu Yizhi, Yu Jianxin, Sun Yi, Xie Weili
College of materials, Shanghai Dianji University, Shanghai 200000, China.
Department of Astronautic Science and Mechanics, Harbin Institute of Technology, Harbin 150000, China.
Polymers (Basel). 2020 Feb 20;12(2):478. doi: 10.3390/polym12020478.
Various amounts of methacryl polyhedral oligomeric silsesquioxane (POSS) were explored to be incorporated into novel nano SiO dental resin composites using light curing method. The scanning electron microscopy (SEM), optical microscopy, fourier transform infrared spectroscopy (FTIR), nanoindentation, nanoscratch and three-point flexure tests were performed. The volumetric shrinkage and mechanical properties such as hardness, elastic modulus, resistance, flexural strength and fracture energy were analyzed. With the additions of POSS, the volume shrinkage decreased and the mechanical properties initially increased. The effects of POSS on these properties were studied to provide a reference for clinically selecting a composite resin with excellent properties.
采用光固化法,将不同量的甲基丙烯酸酯基多面体低聚倍半硅氧烷(POSS)掺入新型纳米SiO₂牙科树脂复合材料中。进行了扫描电子显微镜(SEM)、光学显微镜、傅里叶变换红外光谱(FTIR)、纳米压痕、纳米划痕和三点弯曲试验。分析了体积收缩率以及硬度、弹性模量、阻力、弯曲强度和断裂能等力学性能。随着POSS的添加,体积收缩率降低,力学性能最初有所提高。研究了POSS对这些性能的影响,为临床选择性能优异的复合树脂提供参考。