Blau P J
Blau Tribology Consulting, P.O. Box 631, Enka, NC 28728, USA.
Wear. 2017 Apr 15;376:1830-1840. doi: 10.1016/j.wear.2016.11.012. Epub 2016 Nov 22.
Contrary to the established principles of the scientific method, a surprising number of experimentally-based papers submitted to tribology journals and conferences report only one test result for each material pair or set of applied conditions. However, like hardness, yield strength, fatigue life, and other material properties, wear data exhibit varying degrees of repeatability and reproducibility (R/R). Repeatability concerns the replication of experiments within the same laboratory using the same equipment and materials. Reproducibility concerns testing on different equipment, usually at a different location, but using the same lot of specimens and procedures. An important question is: How many replicate measurements are needed to validate trends in wear behavior or to relatively rank materials, surface treatments, or lubricants? Without repeatability information, it is virtually impossible to establish whether reported material rankings or the effects of variables are real or fall within normal data scatter. The purpose of this paper is to characterize and analyze the R/R of wear data that result from a variety of sources, including material homogeneity, choice of units of measure, and choice of experimental variables. Case studies compare R/R for different forms of wear and their test methods, including ASTM standards. Lessons learned are presented for five forms of wear: (1) cavitation erosion, (2) three-body abrasion, (3) solid particle erosion, (4) dry sliding wear, and (5) fuel lubricity using the ball-on-cylinder (BOCLE) test. Wear transitions can also affect R/R. These examples provide insights for validating wear models, deciding how many repeated tests to make, and when ranking wear-resistance.
与科学方法的既定原则相反,提交给摩擦学期刊和会议的大量基于实验的论文,对于每对材料或每组应用条件仅报告一个测试结果。然而,与硬度、屈服强度、疲劳寿命及其他材料性能一样,磨损数据也表现出不同程度的重复性和再现性(R/R)。重复性涉及在同一实验室使用相同设备和材料对实验进行复制。再现性涉及在不同设备上进行测试,通常是在不同地点,但使用相同批次的试样和程序。一个重要的问题是:需要进行多少次重复测量才能验证磨损行为的趋势,或对材料、表面处理或润滑剂进行相对排名?如果没有重复性信息,几乎不可能确定所报告的材料排名或变量的影响是真实的,还是在正常数据分散范围内。本文的目的是表征和分析来自各种来源的磨损数据的R/R,这些来源包括材料均匀性、测量单位的选择以及实验变量的选择。案例研究比较了不同形式磨损及其测试方法(包括ASTM标准)的R/R。针对五种磨损形式给出了经验教训:(1)空蚀,(2)三体磨料磨损,(3)固体颗粒冲蚀,(4)干滑动磨损,以及(5)使用圆柱-球磨损试验(BOCLE)的燃料润滑性。磨损转变也会影响R/R。这些例子为验证磨损模型、决定进行多少次重复测试以及何时对耐磨性进行排名提供了见解。