Université Côte d'Azur, CNRS, Institut de Chimie de Nice UMR 7272, Nice, France.
Phytochem Anal. 2020 Nov;31(6):778-785. doi: 10.1002/pca.2942. Epub 2020 Apr 26.
In situ analysis of volatile organic compounds (VOCs) emitted by plants is an important challenge in chemical ecology. The traditional approach usually consists in trapping compounds using dynamic headspace extraction (DHS) in-field, followed by gas chromatography analysis coupled with mass spectrometry (GC-MS and/or GC-FID) in the laboratory.
In this study, we evaluated the use of the new portable Torion T-9 GC-MS system for rapid and in situ analysis of VOCs emitted by fine lavender and lavandin species.
All field analyses were performed using a person-portable low-thermal mass GC system coupled with a miniature toroidal ion trap mass analyser (ppGC-ITMS): Torion T-9 portable GC-MS. Subsequently, multivariate statistical analyses were performed to determine chemical differences between species.
Thirty compounds were separated and detected in all lavender above-ground samples in only 3 min of analysis.
The portable GC-MS device enabled a rapid in-field distinction of Lavandula species based on their detected volatile profiles.
原位分析植物挥发的有机化合物(VOCs)是化学生态学的一个重要挑战。传统方法通常包括使用动态顶空提取(DHS)在野外捕集化合物,然后在实验室中进行气相色谱分析,结合质谱法(GC-MS 和/或 GC-FID)。
本研究评估了新型便携式 Torion T-9 GC-MS 系统在快速原位分析精细薰衣草和薰衣草物种挥发的 VOCs 的应用。
所有现场分析均使用与人身尺寸相当的低热质量 GC 系统与微型环形离子阱质谱仪(ppGC-ITMS)耦合:Torion T-9 便携式 GC-MS。随后,进行多元统计分析以确定物种之间的化学差异。
在仅 3 分钟的分析时间内,从所有薰衣草地上部分样本中分离和检测到 30 种化合物。
便携式 GC-MS 设备可根据检测到的挥发性图谱快速区分薰衣草物种。