Mohammadzadeh Behzad, Jung Sunghoon, Lee Tae Hyung, Le Quyet Van, Cha Joo Hwan, Jang Ho Won, Lee Sea-Hoon, Kang Junsuk, Shokouhimehr Mohammadreza
Department of Landscape Architecture and Rural Systems Engineering, Seoul National University, Seoul 08826, Korea.
Research Institute of Agriculture and Life Sciences, Seoul National University, Seoul 08826, Korea.
Materials (Basel). 2020 May 12;13(10):2213. doi: 10.3390/ma13102213.
This study presents a new ultra-high temperature composite fabricated by using zirconium diboride (ZrB), silicon carbide (SiC), and tantalum carbide (TaC) with the volume ratios of 70%, 20%, and 10%, respectively. To attain this novel composite, an advanced processing technique of spark plasma sintering (SPS) was applied to produce ZrB-SiC-TaC. The SPS manufacturing process was achieved under pressure of 30 MPa, at 2000 °C for 5 min. The micro/nanostructure and mechanical characteristics of the composite were clarified using X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), and nano-indentation. For further investigations of the product and its characteristics, X-ray fluorescence (XRF) analysis and X-ray photoelectron spectroscopy (XPS) were undertaken, and the main constituting components were provided. The composite was densified to obtain a fully-dense ternary; the oxide pollutions were wiped out. The mean values of 23,356; 403.5 GPa; and 3100 °C were obtained for the rigidity, elastic modulus, and thermal resistance of the ZrB-SiC-TaC interface, respectively. To explore the practical application of the composite, the natural frequency of an aircraft wing considering three cases of materials: i) with a leading edge made of ZrB-SiC-TaC; ii) the whole wing made of ZrB-SiC-TaC; and iii) the whole wing made of aluminum 2024-T3 were investigated employing a numerical finite element model (FEM) tool ABAQUS and compared with that of a wing of traditional materials. The precision of the method was verified by performing static analysis to obtain the responses of the wing including total deformation, equivalent stress, and strain. A comparison study of the results of this study and published literature clarified the validity of the FEM analysis of the current research. The composite produced in this study significantly can improve the vibrational responses and structural behavior of the aircraft's wings.
本研究展示了一种新型超高温复合材料,它由二硼化锆(ZrB)、碳化硅(SiC)和碳化钽(TaC)制成,其体积比分别为70%、20%和10%。为制备这种新型复合材料,采用了先进的放电等离子烧结(SPS)加工技术来生产ZrB-SiC-TaC。SPS制造过程是在30 MPa的压力、2000 °C的温度下持续5分钟完成的。使用X射线衍射(XRD)、场发射扫描电子显微镜(FESEM)和纳米压痕技术来阐明该复合材料的微观/纳米结构及力学特性。为进一步研究该产品及其特性,进行了X射线荧光(XRF)分析和X射线光电子能谱(XPS)分析,并给出了主要组成成分。该复合材料经过致密化处理以获得完全致密的三元材料;消除了氧化物污染。ZrB-SiC-TaC界面的刚度、弹性模量和热阻的平均值分别为23356、403.5 GPa和3100 °C。为探索该复合材料的实际应用,使用数值有限元模型(FEM)工具ABAQUS研究了飞机机翼在三种材料情况下的固有频率:i)前缘采用ZrB-SiC-TaC;ii)整个机翼采用ZrB-SiC-TaC;iii)整个机翼采用2024-T3铝合金,并与传统材料机翼的固有频率进行了比较。通过进行静态分析以获得机翼的响应,包括总变形、等效应力和应变,验证了该方法的精度。本研究结果与已发表文献的对比研究阐明了当前研究有限元分析的有效性。本研究中制备的复合材料能够显著改善飞机机翼的振动响应和结构性能。